1,3-Benzenedicarboxylic acid, 5-acetyl-

Base Information

Chemical Name:1,3-Benzenedicarboxylic acid, 5-acetyl-
CAS No.:90771-96-3
Molecular Formula:C10H8O5
Molecular Weight:208.171
Hs Code.:

Synonyms:

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Chemical Property of 1,3-Benzenedicarboxylic acid, 5-acetyl-

Chemical Property:

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Technology Process of 1,3-Benzenedicarboxylic acid, 5-acetyl-

There total 9 articles about 1,3-Benzenedicarboxylic acid, 5-acetyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 90909-67-4
dimethyl 5-acetylbenzene-1,3-dicarboxylate

: 90771-96-3
5-Acetylisophthalsaeure

Guidance literature:: With sodium hydroxide; In methanol; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 779-90-8
1,3,5-triacetylbenzene

: 90771-96-3
5-Acetylisophthalsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / TsOH / benzene / 4 h / Heating

2: 1) aq. KOBr, 2) K₂S₂O₅, aq. HCl / 1) dioxane, 0 deg C, 1 h; r.t., 2 h

With hydrogenchloride; potassium disulphite; potassium hypobromite; toluene-4-sulfonic acid; In benzene;

Reference yield:

: 2672-58-4
1,3,5-tris-(methoxycarbonyl)benzene

: 90771-96-3
5-Acetylisophthalsaeure

Guidance literature:: Multi-step reaction with 5 steps

1: lithium borohydride / tetrahydrofuran / 0 °C / Inert atmosphere; Reflux

2: dicyclohexyl-carbodiimide / dichloromethane / Inert atmosphere; Reflux

3: tetrahydrofuran; diethyl ether / 2.5 h / 0 °C / Inert atmosphere

4: dicyclohexyl-carbodiimide / dichloromethane / Inert atmosphere; Reflux

5: sodium hydroxide / methanol / 0 - 20 °C / Inert atmosphere

With lithium borohydride; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; diethyl ether; dichloromethane;