Dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-2(3H)-furanone hydrochloride

Base Information

Chemical Name:Dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-2(3H)-furanone hydrochloride
CAS No.:77694-17-8
Molecular Formula:C₁₃H₁₇NO₂*ClH
Molecular Weight:255.744
Hs Code.:2932209090
DSSTox Substance ID:DTXSID70998884
Mol file:77694-17-8.mol

Synonyms:77694-17-8;Dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-2(3H)-furanone hydrochloride;2(3H)-Furanone, dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-, hydrochloride;DTXSID70998884;LS-70437;3-(Benzylamino)-5,5-dimethyloxolan-2-one--hydrogen chloride (1/1)

Suppliers and Price of Dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-2(3H)-furanone hydrochloride

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2(3H)-FURANONE, DIHYDRO-5,5-DIMETHYL-3-((PHENYLMETHYL)AMINO)-, HYDROCH LORIDE 95.00%
5MG
$ 499.57

Total 2 raw suppliers

Chemical Property of Dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-2(3H)-furanone hydrochloride

Chemical Property:

Vapor Pressure:1.55E-05mmHg at 25°C
Boiling Point:365.6°C at 760 mmHg
Flash Point:174.9°C
PSA：38.33000
LogP:3.06320
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:255.1026065
Heavy Atom Count:17
Complexity:257

Purity/Quality:

99% ^*data from raw suppliers

2(3H)-FURANONE, DIHYDRO-5,5-DIMETHYL-3-((PHENYLMETHYL)AMINO)-, HYDROCH LORIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CC(C(=O)O1)NCC2=CC=CC=C2)C.Cl

Technology Process of Dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-2(3H)-furanone hydrochloride

There total 4 articles about Dihydro-5,5-dimethyl-3-((phenylmethyl)amino)-2(3H)-furanone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 107-86-8
3,3-dimethyl acrylaldehyde

: 77694-17-8
2-(benzylamino)-5,5-dimethylbutyrolactone hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h

2: CH₂Cl₂ / 1 h

3: concd.HCl / 18 h / Heating

With hydrogenchloride; 4 A molecular sieve; In dichloromethane;
DOI:10.1021/jo00188a026

Reference yield:

: 111865-48-6
N-benzyl-(3-methylbut-2-enylidene)amine

: 77694-17-8
2-(benzylamino)-5,5-dimethylbutyrolactone hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 1 h

2: concd.HCl / 18 h / Heating

With hydrogenchloride; In dichloromethane;
DOI:10.1021/jo00188a026

Reference yield:

: 100-46-9
benzylamine

: 77694-17-8
2-(benzylamino)-5,5-dimethylbutyrolactone hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 4 Angstroem molecular sieves / CH₂Cl₂ / 1 h

2: CH₂Cl₂ / 1 h

3: concd.HCl / 18 h / Heating

With hydrogenchloride; 4 A molecular sieve; In dichloromethane;
DOI:10.1021/jo00188a026