Benzenesulfonic acid, (chlorophenylmethylene)ethylhydrazide

Base Information

Chemical Name:Benzenesulfonic acid, (chlorophenylmethylene)ethylhydrazide
CAS No.:90959-30-1
Molecular Formula:C15H15ClN2O2S
Molecular Weight:322.815
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonic acid, (chlorophenylmethylene)ethylhydrazide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenesulfonic acid, (chlorophenylmethylene)ethylhydrazide

There total 2 articles about Benzenesulfonic acid, (chlorophenylmethylene)ethylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 90959-49-2
1-benzoyl-2-ethyl-2-phenylsulfonylhydrazine

: 90959-30-1
N-ethyl-N-(phenylsulfonyl)benzohydrazonoyl chloride

Guidance literature:: With thionyl chloride; for 3h; Heating;
DOI:10.1246/bcsj.57.544

Reference yield:

: 6631-28-3
N-benzenesulfonyl-N'-benzoylhydrazine

: 90959-30-1
N-ethyl-N-(phenylsulfonyl)benzohydrazonoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / NaH / dimethylformamide / 1 h / Ambient temperature

2: 72 percent / thionyl chloride / 3 h / Heating

With thionyl chloride; sodium hydride; In N,N-dimethyl-formamide;
DOI:10.1246/bcsj.57.544