Benz[a]anthracen-2-ol, 1,2,3,4-tetrahydro-, (S)-

Base Information

Chemical Name:Benz[a]anthracen-2-ol, 1,2,3,4-tetrahydro-, (S)-
CAS No.:90997-22-1
Molecular Formula:C₁₈H₁₆O
Molecular Weight:248.324
Hs Code.:

Synonyms:

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Chemical Property of Benz[a]anthracen-2-ol, 1,2,3,4-tetrahydro-, (S)-

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Technology Process of Benz[a]anthracen-2-ol, 1,2,3,4-tetrahydro-, (S)-

There total 8 articles about Benz[a]anthracen-2-ol, 1,2,3,4-tetrahydro-, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 89618-16-6
(+)-(1R,2S)-1,2-Epoxy-1,2,3,4-tetrahydrobenz anthracene

: 90997-22-1,94903-84-1
(-)-(2S)-2-hydroxy-1,2,3,4-tetrahydrobenz anthracene

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1039/P19840000839

Reference yield:

: 57652-74-1
3,4-dihydrobenz anthracen-1(2H)-one

: 90997-22-1,94903-84-1
(-)-(2S)-2-hydroxy-1,2,3,4-tetrahydrobenz anthracene

Guidance literature:: Multi-step reaction with 8 steps

1: 93 percent / sodium borohydride / methanol / 4 h / Ambient temperature

2: 74 percent / toluene-p-sulphonic acid / benzene / 0.5 h / Heating

3: 62 percent / lithium acetate, / acetic acid / 0.75 h / Ambient temperature

4: 75 percent / diborane / tetrahydrofuran

5: pyridine

6: 66 percent / N-bromosuccinimide / CCl₄ / Heating

7: NaOMe / tetrahydrofuran / 0 °C

8: 62 percent / LiAlH₄ / diethyl ether

With sodium tetrahydroborate; N-Bromosuccinimide; lithium aluminium tetrahydride; lithium acetate; sodium methylate; toluene-4-sulfonic acid; diborane; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; acetic acid; benzene;
DOI:10.1039/P19840000839

Reference yield:

: 60968-00-5
(+/-)-1-hydroxy-1,2,3,4-tetrahydrobenz anthracene

: 90997-22-1,94903-84-1
(-)-(2S)-2-hydroxy-1,2,3,4-tetrahydrobenz anthracene

Guidance literature:: Multi-step reaction with 7 steps

1: 74 percent / toluene-p-sulphonic acid / benzene / 0.5 h / Heating

2: 62 percent / lithium acetate, / acetic acid / 0.75 h / Ambient temperature

3: 75 percent / diborane / tetrahydrofuran

4: pyridine

5: 66 percent / N-bromosuccinimide / CCl₄ / Heating

6: NaOMe / tetrahydrofuran / 0 °C

7: 62 percent / LiAlH₄ / diethyl ether

With N-Bromosuccinimide; lithium aluminium tetrahydride; lithium acetate; sodium methylate; toluene-4-sulfonic acid; diborane; In tetrahydrofuran; pyridine; tetrachloromethane; diethyl ether; acetic acid; benzene;
DOI:10.1039/P19840000839