Ergoline-8-methanol, 8,9-didehydro-6-methyl-

Base Information

Chemical Name:Ergoline-8-methanol, 8,9-didehydro-6-methyl-
CAS No.:91106-37-5
Molecular Formula:C₁₆H₁₈N₂O
Molecular Weight:254.332
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ergoline-8-methanol, 8,9-didehydro-6-methyl-

Chemical Property:

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Technology Process of Ergoline-8-methanol, 8,9-didehydro-6-methyl-

There total 6 articles about Ergoline-8-methanol, 8,9-didehydro-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 91106-36-4
(3β)-2,3-Dihydroelymoclavine

: 548-43-6,91106-37-5
(+/-)-Elymoclavine

Guidance literature:: With indole; benzeneseleninic anhydride; In tetrahydrofuran; at 40 ℃; for 1.5h;

Reference yield:

: 84936-67-4,84986-20-9,98633-52-4
(3aβ,5aβ,6aβ,11bα,11cβ)-8-benzoyl-5,5a,6,6a,7,8,11b,11c-octahydro-5-methylfuro<3,2-c>indolo<4,3-fg>quinolin-4(3aH)-one

: 548-43-6,91106-37-5
(+/-)-Elymoclavine

Guidance literature:: Multi-step reaction with 5 steps

1: 1) ozone, 2) LiAlH₄ / 1) CHCl₃, 2) diethylether, THF, 2 h, reflux

2: 89 percent / pyridine / 0 °C

3: 18 percent / SOCl₂ / benzene / 1 h / Heating

4: 66 percent / conc. HCl / methanol / Heating

5: 94 percent / benzeneseleninic anhydride, indole / tetrahydrofuran / 1.5 h / 40 °C

With pyridine; indole; hydrogenchloride; lithium aluminium tetrahydride; thionyl chloride; benzeneseleninic anhydride; ozone; In tetrahydrofuran; methanol; benzene;

Reference yield:

: 91106-44-4,91177-61-6
(3β,8α,9α)-1-Benzyl-2,3-dihydro-8-hydroxymethyl-6-methylergolin-9-ol

: 548-43-6,91106-37-5
(+/-)-Elymoclavine

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / H₂, 10percent aq. HCl, 70percent HClO₄ / 40percent Pd/C / 4 h / 3420 Torr

2: 89 percent / pyridine / 0 °C

3: 18 percent / SOCl₂ / benzene / 1 h / Heating

4: 66 percent / conc. HCl / methanol / Heating

5: 94 percent / benzeneseleninic anhydride, indole / tetrahydrofuran / 1.5 h / 40 °C

With pyridine; indole; hydrogenchloride; thionyl chloride; perchloric acid; benzeneseleninic anhydride; hydrogen; palladium on activated charcoal; In tetrahydrofuran; methanol; benzene;