hunterioside

Base Information

Chemical Name:hunterioside
CAS No.:156431-08-2
Molecular Formula:C₃₂H₄₂N₂O₁₄
Molecular Weight:678.69
Hs Code.:

Synonyms:2H-Pyran-5-carboxylicacid, 3-ethenyl-2-[(6-O-a-D-glucopyranosyl-b-D-glucopyranosyl)oxy]-3,4-dihydro-4-[(2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indol-1-yl)methyl]-,[2S-[2a,3b,4b(R*)]]-; Hunterioside

Suppliers and Price of hunterioside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of hunterioside

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:961°Cat760mmHg
PKA:4.67±0.70(Predicted)
Flash Point:535°C
PSA：252.88000
Density:1.59g/cm³
LogP:-1.54250

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of hunterioside

There total 13 articles about hunterioside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 496-42-4
1H-indole-2-ethanamine

: 233661-57-9
(4aS,5R,6S)-3-Methoxy-6-[(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-hydroxymethyl-tetrahydro-pyran-2-yloxymethyl)-tetrahydro-pyran-2-yloxy]-5-vinyl-4,4a,5,6-tetrahydro-3H-pyrano[3,4-c]pyran-1-one

: 156431-08-2
hunterioside

Guidance literature:: In water; acetic acid; at 20 ℃;
DOI:10.1016/S0040-4039(99)00928-4

Reference yield:

: 19351-63-4
secologanin

: 156431-08-2
hunterioside

Guidance literature:: Multi-step reaction with 8 steps

1: 72 percent / DMAP / dimethylformamide / 20 °C

2: 83 percent / pyridine / CH₂Cl₂

3: 76 percent / Amberlite IR 120B; Na₂SO₄ / acetonitrile / 5 °C

4: 82 percent / TBAF; AcOH / tetrahydrofuran / 0 °C

5: 82 percent / TrClO₄ / CH₂Cl₂; diethyl ether

6: 81 percent / AcOH; H₂O / Heating

7: 86 percent / K₂CO₃ / methanol

8: 24 percent / acetic acid; H₂O / 20 °C

With pyridine; dmap; Cl⁽³⁾HO₄; Amberlite IR 120B; tetrabutyl ammonium fluoride; water; potassium carbonate; acetic acid; sodium sulfate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetonitrile; 1: Etherification / 2: Acetylation / 3: Etherification / 4: Hydrolysis / 5: Substitution / 6: Hydrolysis / 7: Hydrolysis / 8: Condensation;
DOI:10.1016/S0040-4039(99)00928-4

Reference yield:

: 36215-42-6,52389-39-6
N-<3,4,6-tri-O-acetyl-β-D-glucopyranosyl>piperidine

: 156431-08-2
hunterioside

Guidance literature:: Multi-step reaction with 7 steps

1: 97 percent / imidazole / dimethylformamide / 20 °C

2: 85 percent / AcOH; H₂O / acetone / Heating

3: 84 percent / DBU / CH₂Cl₂

4: 82 percent / TrClO₄ / CH₂Cl₂; diethyl ether

5: 81 percent / AcOH; H₂O / Heating

6: 86 percent / K₂CO₃ / methanol

7: 24 percent / acetic acid; H₂O / 20 °C

With 1H-imidazole; Cl⁽³⁾HO₄; water; potassium carbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; diethyl ether; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; 1: Etherification / 2: Hydrolysis / 3: Esterification / 4: Substitution / 5: Hydrolysis / 6: Hydrolysis / 7: Condensation;
DOI:10.1016/S0040-4039(99)00928-4