(E)-3-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylidene)propionic acid S-oxide

Base Information

Chemical Name:(E)-3-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylidene)propionic acid S-oxide
CAS No.:112930-62-8
Molecular Formula:C₁₇H₁₄O₃S
Molecular Weight:298.362
Hs Code.:
Nikkaji Number:J316.126I

Synonyms:BRN 3617699;Propanoic acid, 3-dibenzo(b,e)thiepin-11(6H)-ylidene-, S-oxide, (E)-;(E)-3-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylidene)propionic acid S-oxide;112930-62-8;LS-121345;(E)-3-[(6,11-Dihydrodibenzo[b,e]thiepin 5-oxide)-11-ylidene]propionic acid

Suppliers and Price of (E)-3-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylidene)propionic acid S-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylidene)propionic acid S-oxide

Chemical Property:

Vapor Pressure:6.35E-15mmHg at 25°C
Boiling Point:593.3°Cat760mmHg
Flash Point:312.6°C
Density:1.41g/cm³
XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:298.06636548
Heavy Atom Count:21
Complexity:457

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C(=CCC(=O)O)C3=CC=CC=C3S1=O
Isomeric SMILES:C1C2=CC=CC=C2/C(=C\CC(=O)O)/C3=CC=CC=C3S1=O

Technology Process of (E)-3-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylidene)propionic acid S-oxide

There total 8 articles about (E)-3-(6,11-Dihydrodibenzo(b,e)thiepin-11-ylidene)propionic acid S-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 112930-58-2
(E)-3-(6,11-dihydrodibenzothiepin-11-ylidene)propionic acid

: 112930-62-8
(E)-11-(2-Carboxyethylidene)-6,11-dihydrodibenzothiepin 5-Oxide

Guidance literature:: With dihydrogen peroxide; In acetic acid; for 1h; Ambient temperature;

Reference yield:

: 1531-77-7
dibenzo[b,e]thiepin-11(6H)-one

: 112930-62-8
(E)-11-(2-Carboxyethylidene)-6,11-dihydrodibenzothiepin 5-Oxide

Guidance literature:: Multi-step reaction with 5 steps

1: 1) Mg / in THF

2: 94 percent / HBr / acetic acid / 1 h / 15 °C

3: 80 percent / tetrahydrofuran; ethanol; H₂O / 1.5 h / Ambient temperature

4: aq. KOH / ethanol / 3.5 h / Heating

5: 88 percent / 30percent H₂O₂ / acetic acid / 1 h / Ambient temperature

With potassium hydroxide; hydrogen bromide; dihydrogen peroxide; magnesium; In tetrahydrofuran; ethanol; water; acetic acid;

Reference yield:

: 112930-52-6
6,11-Dihydro-11-vinyldibenzothiepin-11-ol

: 112930-62-8
(E)-11-(2-Carboxyethylidene)-6,11-dihydrodibenzothiepin 5-Oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / HBr / acetic acid / 1 h / 15 °C

2: 80 percent / tetrahydrofuran; ethanol; H₂O / 1.5 h / Ambient temperature

3: aq. KOH / ethanol / 3.5 h / Heating

4: 88 percent / 30percent H₂O₂ / acetic acid / 1 h / Ambient temperature

With potassium hydroxide; hydrogen bromide; dihydrogen peroxide; In tetrahydrofuran; ethanol; water; acetic acid;