1-[(2R,5S,9R)-9-Bromo-6,10,10-trimethylspiro[4.5]dec-6-en-2-yl]ethanone

Base Information

Chemical Name:1-[(2R,5S,9R)-9-Bromo-6,10,10-trimethylspiro[4.5]dec-6-en-2-yl]ethanone
CAS No.:30925-25-8
Molecular Formula:C₁₅H₂₃BrO
Molecular Weight:299.251
Hs Code.:
Mol file:30925-25-8.mol

Synonyms:Ethanone,1-(9-bromo-6,10,10-trimethylspiro[4.5]dec-6-en-2-yl)-, [2R-[2a,5a(R*)]]-; Spiro[4.5]decane, ethanone deriv.;Spirolaurenone

Suppliers and Price of 1-[(2R,5S,9R)-9-Bromo-6,10,10-trimethylspiro[4.5]dec-6-en-2-yl]ethanone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 1-[(2R,5S,9R)-9-Bromo-6,10,10-trimethylspiro[4.5]dec-6-en-2-yl]ethanone

Chemical Property:

PSA：17.07000
LogP:4.50160

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-[(2R,5S,9R)-9-Bromo-6,10,10-trimethylspiro[4.5]dec-6-en-2-yl]ethanone

There total 8 articles about 1-[(2R,5S,9R)-9-Bromo-6,10,10-trimethylspiro[4.5]dec-6-en-2-yl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76235-51-3
1-((2S,5R,9S)-9-Bromo-6,10,10-trimethyl-spiro[4.5]dec-6-en-2-yl)-ethanol

: 30925-25-8,83680-06-2
(+/-)-spirolaurenone

Guidance literature:: With jones reagent; In acetone; at 0 ℃; for 0.166667h; Yield given;
DOI:10.1016/S0040-4039(00)88440-3

Reference yield:

: 54278-86-3
glanduliferol

: 30925-25-8,83680-06-2
spirolaurenone

Guidance literature:: With silver(l) oxide; In hexane; at 50 ℃; for 0.25h;
DOI:10.1016/S0040-4020(01)83121-5

Reference yield:

: 83637-76-7
(2S,5R,9S)-9-Bromo-6,10,10-trimethyl-spiro[4.5]dec-6-ene-2-carbaldehyde

: 30925-25-8,83680-06-2
(+/-)-spirolaurenone

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether / 0.17 h / -15 °C

2: Jones reagent / acetone / 0.17 h / 0 °C

With jones reagent; In diethyl ether; acetone;
DOI:10.1016/S0040-4039(00)88440-3