4-Tert-butyl-1-[(2,2-dichlorocyclopropyl)methyl]-2-nitrobenzene

Base Information

Chemical Name:4-Tert-butyl-1-[(2,2-dichlorocyclopropyl)methyl]-2-nitrobenzene
CAS No.:5216-30-8
Molecular Formula:C14H8 Cl2
Molecular Weight:247.124
Hs Code.:
DSSTox Substance ID:DTXSID90385393
Mol file:5216-30-8.mol

Synonyms:5216-30-8;4-tert-butyl-1-[(2,2-dichlorocyclopropyl)methyl]-2-nitrobenzene;CBMicro_014258;DTXSID90385393;SMSF0004649;BIM-0014171.P001;Benzene, 1,1'-(1,2-ethynediyl)bis[3-chloro-

Suppliers and Price of 4-Tert-butyl-1-[(2,2-dichlorocyclopropyl)methyl]-2-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Biosynth Carbosynth
3,3'-Dichlorodiphenylacetylene
2 g
$ 250.00

Biosynth Carbosynth
3,3'-Dichlorodiphenylacetylene
1 g
$ 150.00

Biosynth Carbosynth
3,3'-Dichlorodiphenylacetylene
250 mg
$ 50.00

American Custom Chemicals Corporation
1,1'-(1,2-ETHYNEDIYL)BIS[3-CHLORO-BENZENE 95.00%
5MG
$ 499.24

Total 1 raw suppliers

Chemical Property of 4-Tert-butyl-1-[(2,2-dichlorocyclopropyl)methyl]-2-nitrobenzene

Chemical Property:

Vapor Pressure:1.87E-05mmHg at 25°C
Melting Point:81-82 °C
Boiling Point:373.9°Cat760mmHg
Flash Point:179.9°C
PSA：45.82000
Density:1.26g/cm³
LogP:5.15180
XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:301.0636342
Heavy Atom Count:19
Complexity:359

Purity/Quality:

99% ^*data from raw suppliers

3,3'-Dichlorodiphenylacetylene ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=C(C=C1)CC2CC2(Cl)Cl)[N+](=O)[O-]

Technology Process of 4-Tert-butyl-1-[(2,2-dichlorocyclopropyl)methyl]-2-nitrobenzene

There total 18 articles about 4-Tert-butyl-1-[(2,2-dichlorocyclopropyl)methyl]-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 5216-30-8
1,2-bis(3-chlorophenyl)ethyne

Guidance literature:: With tris[2-(dimethylamino)ethyl]amine; copper; In tetrahydrofuran; at 60 ℃; for 5h; Schlenk technique; Inert atmosphere;

Reference yield: 97.0%

: 625-99-0
3-iodochlorobenzene

: 74-86-2,25067-58-7
acetylene

: 5216-30-8
1,2-bis(3-chlorophenyl)ethyne

Guidance literature:: With triethylamine; copper(l) iodide; In N,N-dimethyl-formamide; at 30 ℃; for 12h;
DOI:10.1039/P19960000449

Reference yield: 93.0%

: 625-99-0
3-iodochlorobenzene

: 1066-54-2
trimethylsilylacetylene

: 5216-30-8
1,2-bis(3-chlorophenyl)ethyne

Guidance literature:: With copper(l) iodide; water; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis-triphenylphosphine-palladium(II) chloride; In benzene; at 20 ℃; for 18h;
DOI:10.1021/ol026266n