Tetramethyldistiboxane

Base Information

Chemical Name:Tetramethyldistiboxane
CAS No.:73513-49-2
Molecular Formula:C₄H₁₂OSb₂
Molecular Weight:319.639
Hs Code.:
DSSTox Substance ID:DTXSID80586751
NSC Number:369733
Wikidata:Q82478945

Synonyms:73513-49-2;Tetramethyldistiboxane;bis(dimethylstibino) oxide;DTXSID80586751;NSC369733;NSC-369733

Suppliers and Price of Tetramethyldistiboxane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of Tetramethyldistiboxane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:319.89684
Heavy Atom Count:7
Complexity:39

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Sb](C)O[Sb](C)C

Technology Process of Tetramethyldistiboxane

There total 2 articles about Tetramethyldistiboxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.7%

: 7732-18-5
water

: 53234-94-9
dimethylantimony bromide

: 73513-49-2
bis(dimethylantimony) oxide

Guidance literature:: In sodium hydroxide; aq. NaOH; room temp., under Ar, Me2SbBr was added dropwise to aq. NaOH soln., stirring for 2 h at room temp.,; extn. with petroleum ether, soln. was dried over anhyd. Na2SO4, solventwas removed, repeated distn. at 57.5-58.5 °C/7mbar, purity was 98.5 %;
DOI:10.1002/1521-3749(200007)626:7<1595::AID-ZAAC1595>3.0.CO;2-Q