Hydrazinecarboxylic acid, 2-[5-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]-2-[[[(4- methoxyphenyl)methoxy]carbonyl]amino]-1-oxopentyl]-, 2,2,2-trichloroethyl ester, (S)-

Base Information

Chemical Name:Hydrazinecarboxylic acid, 2-[5-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]-2-[[[(4- methoxyphenyl)methoxy]carbonyl]amino]-1-oxopentyl]-, 2,2,2-trichloroethyl ester, (S)-
CAS No.:91474-60-1
Molecular Formula:C₂₇H₃₅Cl₃N₆O₈S
Molecular Weight:710.035
Hs Code.:

Hydrazinecarboxylic acid,
2-[5-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]-2-[[[(4-
methoxyphenyl)methoxy]carbonyl]amino]-1-oxopentyl]-,
2,2,2-trichloroethyl ester, (S)-

Synonyms:

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Chemical Property of Hydrazinecarboxylic acid, 2-[5-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]-2-[[[(4- methoxyphenyl)methoxy]carbonyl]amino]-1-oxopentyl]-, 2,2,2-trichloroethyl ester, (S)-

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Technology Process of Hydrazinecarboxylic acid, 2-[5-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]-2-[[[(4- methoxyphenyl)methoxy]carbonyl]amino]-1-oxopentyl]-, 2,2,2-trichloroethyl ester, (S)-

There total 1 articles about Hydrazinecarboxylic acid, 2-[5-[[imino[[(2,4,6-trimethylphenyl)sulfonyl]amino]methyl]amino]-2-[[[(4- methoxyphenyl)methoxy]carbonyl]amino]-1-oxopentyl]-, 2,2,2-trichloroethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 31434-96-5
2,2,2-trichloroethyloxycarbonylhydrazine

: 68262-73-7
Z(OMe)-Arg(Mts)-OH

: 91474-60-1
Z(OMe)-Arg(Mts)-NHNH-Troc

Guidance literature:: Yield given. Multistep reaction; 1.) formation of mixed anhydride; 2.) THF, 4 h;

Reference yield: 71.0%

: 108056-94-6
Z(OMe)-Asp(OChp)-OSu

: 91474-60-1
Z(OMe)-Arg(Mts)-NHNH-Troc

: 123197-07-9
Z(OMe)-Asp(OChp)-Arg(Mts)-NHNH-Troc

Guidance literature:: With TEA; methoxybenzene; trifluoroacetic acid; 1.) 60 min; 2.) DMF;
DOI:10.1248/cpb.36.4364

Reference yield:

: 91474-60-1
Z(OMe)-Arg(Mts)-NHNH-Troc

: 123196-88-3
Z(OMe)-Ser-Asp(OChp)-Arg(Mts)-NHNH₂

Guidance literature:: Multi-step reaction with 3 steps

1: 71 percent / 1.) TFA, anisole; 2.) TEA / 1.) 60 min; 2.) DMF

2: 85 percent / 1.) TFA, anisole; 2.) TEA, NMM / 1.) 60 min; 2.) DMF, 40 h

3: 68 percent / Zn / dimethylformamide; acetic acid / 3.5 h

With 4-methyl-morpholine; TEA; methoxybenzene; trifluoroacetic acid; zinc; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1248/cpb.36.4364