Phosphine, [2-(1-methylethyl)phenyl]-

Base Information

Chemical Name:Phosphine, [2-(1-methylethyl)phenyl]-
CAS No.:915199-68-7
Molecular Formula:C9H13P
Molecular Weight:152.176
Hs Code.:

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Chemical Property of Phosphine, [2-(1-methylethyl)phenyl]-

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Technology Process of Phosphine, [2-(1-methylethyl)phenyl]-

There total 7 articles about Phosphine, [2-(1-methylethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1237893-82-1
2-t-BuC₆H₄PCl₂

: 915199-68-7
2-i-PrC₆H₄PH₂

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/hc.20619

Reference yield: 70.0%

: 2-i-PrC₆H₄PCl₂

: 915199-68-7
2-i-PrC₆H₄PH₂

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/hc.20619 DOI:10.1002/hc.20606

Reference yield:

: 643-28-7
2-isopropylaniline

: 915199-68-7
2-i-PrC₆H₄PH₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogen bromide; sodium nitrite / Inert atmosphere

1.2: Inert atmosphere

2.1: magnesium / tetrahydrofuran / 20 °C / Inert atmosphere; Reflux

2.2: 20 °C / Inert atmosphere

3.1: hydrogenchloride / dichloromethane / Inert atmosphere

4.1: lithium aluminium tetrahydride / diethyl ether / -78 - 20 °C / Inert atmosphere

With hydrogenchloride; lithium aluminium tetrahydride; hydrogen bromide; magnesium; sodium nitrite; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Sandmeyer reaction / 1.2: Sandmeyer reaction;
DOI:10.1002/hc.20619