2-(2-bromophenyl)-N-chloro-N-methoxyacetamide

Base Information

Chemical Name:2-(2-bromophenyl)-N-chloro-N-methoxyacetamide
CAS No.:91523-30-7
Molecular Formula:C9H9BrClNO2
Molecular Weight:278.533
Hs Code.:
DSSTox Substance ID:DTXSID20536331
Wikidata:Q82410959

Synonyms:2-(2-bromophenyl)-N-chloro-N-methoxyacetamide;91523-30-7;DTXSID20536331

Suppliers and Price of 2-(2-bromophenyl)-N-chloro-N-methoxyacetamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-(2-bromophenyl)-N-chloro-N-methoxyacetamide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:276.95052
Heavy Atom Count:14
Complexity:203

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CON(C(=O)CC1=CC=CC=C1Br)Cl

Technology Process of 2-(2-bromophenyl)-N-chloro-N-methoxyacetamide

There total 2 articles about 2-(2-bromophenyl)-N-chloro-N-methoxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 121989-40-0
2-(2-bromophenyl)-N-methoxyacetamide

: 91523-30-7
2-(2-bromophenyl)-N-chloro-N-methoxyacetamide

Guidance literature:: With tert-butylhypochlorite; In dichloromethane; at 0 ℃; for 0.333333h;
DOI:10.1021/jo00275a027

Reference yield:

: 55116-09-1
2-bromophenylacetyl chloride

: 91523-30-7
2-(2-bromophenyl)-N-chloro-N-methoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / sodium carbonate / benzene; H₂O / 5 h / Ambient temperature

2: 94 percent / tert-butyl hypochlorite / CH₂Cl₂ / 0.33 h / 0 °C

With tert-butylhypochlorite; sodium carbonate; In dichloromethane; water; benzene;
DOI:10.1021/jo00275a027