3,5-DibroMo-2-chloro-4,6-diMethylpyridine

Base Information

Chemical Name:3,5-DibroMo-2-chloro-4,6-diMethylpyridine
CAS No.:915946-47-3
Molecular Formula:C7H6Br2ClN
Molecular Weight:299.392
Hs Code.:2933399090
Mol file:915946-47-3.mol

Synonyms:

Suppliers and Price of 3,5-DibroMo-2-chloro-4,6-diMethylpyridine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
3,5-Dibromo-2-chloro-4,6-dimethylpyridine 95+%
1g
$ 698.00

Chemenu
3,5-dibromo-2-chloro-4,6-dimethylpyridine 95%
1g
$ 660.00

Total 5 raw suppliers

Chemical Property of 3,5-DibroMo-2-chloro-4,6-diMethylpyridine

Chemical Property:

Melting Point:99-111 °C(Solv: methanol (67-56-1); ethyl acetate (141-78-6))
Boiling Point:296.8±35.0 °C(Predicted)
PKA:-1.25±0.10(Predicted)
PSA：12.89000
Density:1.876±0.06 g/cm3(Predicted)
LogP:3.87680
Storage Temp.:2-8°C

Purity/Quality:

98% ^*data from raw suppliers

3,5-Dibromo-2-chloro-4,6-dimethylpyridine 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-DibroMo-2-chloro-4,6-diMethylpyridine

There total 2 articles about 3,5-DibroMo-2-chloro-4,6-diMethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 857429-63-1
3,5-dibromo-4,6-dimethylpyridin-2(1H)-one

: 915946-47-3
3,5-dibromo-2-chloro-4,6-dimethylpyridine

Guidance literature:: With trichlorophosphate; at 135 ℃; for 8h;
DOI:10.1055/s-2006-942535

Reference yield:

: 16115-08-5
4,6-dimethyl-2-pyridone

: 915946-47-3
3,5-dibromo-2-chloro-4,6-dimethylpyridine

Guidance literature:: Multi-step reaction with 2 steps

1: Br₂; acetic acid / 1 h

2: 79 percent / POCl₃ / 8 h / 135 °C

With bromine; acetic acid; trichlorophosphate;
DOI:10.1055/s-2006-942535

Reference yield: 92.0%

: 915946-47-3
3,5-dibromo-2-chloro-4,6-dimethylpyridine

: 98-80-6
phenylboronic acid

: 101868-36-4
2-chloro-4,6-dimethyl-3,5-diphenylpyridine

Guidance literature:: With palladium diacetate; sodium carbonate; tris-(o-tolyl)phosphine; In ethanol; water; toluene; at 85 ℃; for 8h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere;
DOI:10.3998/ark.5550190.p009.772