Benzenepropanamide, a-(dimethylamino)-N-[2-(1H-indol-3-yl)-2-oxoethyl]-,(aS)-

Base Information

Chemical Name:Benzenepropanamide, a-(dimethylamino)-N-[2-(1H-indol-3-yl)-2-oxoethyl]-,(aS)-
CAS No.:161068-70-8
Molecular Formula:C21H23 N3 O2
Molecular Weight:349.433
Hs Code.:

Synonyms:Benzenepropanamide,a-(dimethylamino)-N-[2-(1H-indol-3-yl)-2-oxoethyl]-,(S)-; Prealmazole C

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Chemical Property of Benzenepropanamide, a-(dimethylamino)-N-[2-(1H-indol-3-yl)-2-oxoethyl]-,(aS)-

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of Benzenepropanamide, a-(dimethylamino)-N-[2-(1H-indol-3-yl)-2-oxoethyl]-,(aS)-

There total 5 articles about Benzenepropanamide, a-(dimethylamino)-N-[2-(1H-indol-3-yl)-2-oxoethyl]-,(aS)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 17469-89-5
(2S)-2-(dimethylamino)-3-phenylpropanoic acid

: 53552-11-7
<2-(1H-indol-3-yl)-2-oxoethyl> ammonium chloride

: 161068-70-8
prealmazole C

Guidance literature:: <2-(1H-indol-3-yl)-2-oxoethyl> ammonium chloride; With triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

(2S)-2-(dimethylamino)-3-phenylpropanoic acid; In tetrahydrofuran; at 0 - 23 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tet.2010.03.109

Reference yield: 80.0%

: 53552-11-7
<2-(1H-indol-3-yl)-2-oxoethyl> ammonium chloride

: (S)-2-Dimethylamino-1-imidazol-1-yl-3-phenyl-propan-1-one

: 161068-70-8
prealmazole C

Guidance literature:: In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1002/hlca.19940770726

Reference yield:

: 703-80-0
3-acetylindole

: 161068-70-8
prealmazole C

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / Br₂ / methanol / 2 h / Heating

2: 98 percent / hexamethylenetetramine / acetone; CHCl₃ / 3 h / Ambient temperature

3: 80 percent / dimethylformamide / Ambient temperature

With hexamethylenetetramine; bromine; In methanol; chloroform; N,N-dimethyl-formamide; acetone;
DOI:10.1002/hlca.19940770726