Bicyclo[2.2.1]heptane-2-carboxylic acid, 2-(acetylamino)-5,6-dihydroxy-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (1S,2S,4R,5R,6S)-

Base Information

Chemical Name:Bicyclo[2.2.1]heptane-2-carboxylic acid, 2-(acetylamino)-5,6-dihydroxy-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (1S,2S,4R,5R,6S)-
CAS No.:915957-03-8
Molecular Formula:C26H37NO5
Molecular Weight:443.583
Hs Code.:

Bicyclo[2.2.1]heptane-2-carboxylic acid,
2-(acetylamino)-5,6-dihydroxy-,
(1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester,
(1S,2S,4R,5R,6S)-

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Chemical Property of Bicyclo[2.2.1]heptane-2-carboxylic acid, 2-(acetylamino)-5,6-dihydroxy-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (1S,2S,4R,5R,6S)-

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Technology Process of Bicyclo[2.2.1]heptane-2-carboxylic acid, 2-(acetylamino)-5,6-dihydroxy-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (1S,2S,4R,5R,6S)-

There total 1 articles about Bicyclo[2.2.1]heptane-2-carboxylic acid, 2-(acetylamino)-5,6-dihydroxy-, (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenylethyl)cyclohexyl ester, (1S,2S,4R,5R,6S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 905733-13-3
(1'R,3'R,4'S)-8'-phenylmenthyl (1R,2S,4R)-2-acetylamino-bicyclo[2.2.1]hept-5-ene-2-carboxylate

: 915957-03-8
(1R,3R,4S)-8-phenylmenthyl (1S,2S,4R,5R,6S)-2-acetylamino-5,6-dihydroxybicyclo[2.2.1]heptane-2-carboxylate

Guidance literature:: With osmium(VIII) oxide; 4-methylmorpholine N-oxide; In water; acetone; at 20 ℃; for 8h;
DOI:10.1021/jo061391o

Reference yield:

: 915957-03-8
(1R,3R,4S)-8-phenylmenthyl (1S,2S,4R,5R,6S)-2-acetylamino-5,6-dihydroxybicyclo[2.2.1]heptane-2-carboxylate

: 915957-07-2
(1R,3R,4S)-8-phenylmenthyl (1S,2S,4R)-1-acetylamino-2,4-diformylcyclopentanecarboxylate

Guidance literature:: With sodium periodate; In 1,4-dioxane; water; at 20 ℃; for 2h;
DOI:10.1021/jo061391o

Reference yield:

: 915957-03-8
(1R,3R,4S)-8-phenylmenthyl (1S,2S,4R,5R,6S)-2-acetylamino-5,6-dihydroxybicyclo[2.2.1]heptane-2-carboxylate

: 915957-22-1
6-amino-3-(4-methoxy-benzyl)-3-aza-bicyclo[3.2.1]octane-6-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 398 mg / sodium periodate / dioxane; H₂O / 2 h / 20 °C

2: 58 percent / NaBH(OAc)3; AcOH / 1,2-dichloro-ethane / 4 h / 25 °C

3: 60 percent / MeONa / methanol / 50 h / 100 °C

With sodium periodate; sodium methylate; sodium tris(acetoxy)borohydride; acetic acid; In 1,4-dioxane; methanol; water; 1,2-dichloro-ethane;
DOI:10.1021/jo061391o