Benzamide, 4-fluoro-N-[(1S)-1-(hydroxymethyl)-2-propen-1-yl]-2-(trifluoromethyl)-

Base Information

Chemical Name:Benzamide, 4-fluoro-N-[(1S)-1-(hydroxymethyl)-2-propen-1-yl]-2-(trifluoromethyl)-
CAS No.:915958-96-2
Molecular Formula:C12H11F4NO2
Molecular Weight:277.218
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzamide, 4-fluoro-N-[(1S)-1-(hydroxymethyl)-2-propen-1-yl]-2-(trifluoromethyl)-

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Technology Process of Benzamide, 4-fluoro-N-[(1S)-1-(hydroxymethyl)-2-propen-1-yl]-2-(trifluoromethyl)-

There total 1 articles about Benzamide, 4-fluoro-N-[(1S)-1-(hydroxymethyl)-2-propen-1-yl]-2-(trifluoromethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 313995-40-3
(2S)-1-hydroxybut-3-en-2-methylpyrrole-2-carboxylate

: 189807-21-4
2-trifluoromethyl-4-fluorobenzoyl chloride

: 915958-96-2
4-fluoro-N-((S)-1-hydroxymethyl-allyl)-2-trifluoromethyl-benzamide

Guidance literature:: (2S)-1-hydroxybut-3-en-2-methylpyrrole-2-carboxylate; 2-trifluoromethyl-4-fluorobenzoyl chloride; With triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h;

With lithium hydroxide; water; In tetrahydrofuran; at 0 - 20 ℃; for 15h;

Reference yield: 92.0%

: 915958-96-2
4-fluoro-N-((S)-1-hydroxymethyl-allyl)-2-trifluoromethyl-benzamide

: 915958-97-3
(S)-2-(4-fluoro-2-trifluoromethyl-benzoylamino)-but-3-enoic acid

Guidance literature:: With chromium(VI) oxide; sodium periodate; periodic acid; In water; acetonitrile; at 0 - 20 ℃; for 18h;

Reference yield:

: 915958-96-2
4-fluoro-N-((S)-1-hydroxymethyl-allyl)-2-trifluoromethyl-benzamide

: 915958-98-4
(S)-2-(4-fluoro-2-trifluoromethyl-benzoylamino)-but-3-enoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: chromium(VI) oxide; sodium periodate; periodic acid / water; acetonitrile / 18 h / 0 - 20 °C

2: thionyl chloride / 72.5 h / 20 °C

With chromium(VI) oxide; sodium periodate; thionyl chloride; periodic acid; In water; acetonitrile;