2-(7-chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-N,N-dimethylethanamine

Base Information

Chemical Name:2-(7-chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-N,N-dimethylethanamine
CAS No.:30490-66-5
Molecular Formula:C₁₉H₂₁ClN₂
Molecular Weight:312.842
Hs Code.:
Mol file:30490-66-5.mol

Synonyms:5H-Dibenz[b,f]azepine,3-chloro-11-[2-(dimethylamino)ethyl]-5-methyl- (8CI); 5H-Dibenz[b,f]azepine-11-ethanamine,3-chloro-N,N,5-trimethyl- (9CI)

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(7-chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-N,N-dimethylethanamine

Chemical Property:

Vapor Pressure:7.9E-08mmHg at 25°C
Boiling Point:436.7°C at 760 mmHg
Flash Point:217.9°C
PSA：6.48000
Density:1.133g/cm³
LogP:4.97860

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(7-chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-N,N-dimethylethanamine

There total 4 articles about 2-(7-chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-N,N-dimethylethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 30490-59-6
[2-chloro-9-(2-dimethylamino-ethyl)-10-methyl-9,10-dihydro-acridin-9-yl]-methanol

: 30490-66-5
[2-(7-Chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-ethyl]-dimethyl-amine

Guidance literature:: With phosphorus pentoxide; In various solvent(s); for 3h; Heating;

Reference yield:

: 30490-57-4
2-chloro-10-methyl-9,10-dihydro-acridine-9-carboxylic acid methyl ester

: 30490-66-5
[2-(7-Chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-ethyl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: ter-BuOK / tetrahydrofuran; hexamethylphosphoric acid triamide / 16 h

2: 89 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

3: 88 percent / P₂O₅ / various solvent(s) / 3 h / Heating

With lithium aluminium tetrahydride; potassium tert-butylate; phosphorus pentoxide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;

Reference yield:

: 30490-58-5
2-chloro-9-methoxycarbonyl-9(β-dimethylaminoethyl)-10-methyl-acridane

: 30490-66-5
[2-(7-Chloro-5-methyl-5H-dibenzo[b,f]azepin-10-yl)-ethyl]-dimethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / LiAlH₄ / tetrahydrofuran / 2 h / Heating

2: 88 percent / P₂O₅ / various solvent(s) / 3 h / Heating

With lithium aluminium tetrahydride; phosphorus pentoxide; In tetrahydrofuran;