9-(4-Chlorobenzylidene)-2-nitro-9h-fluorene

Base Information

Chemical Name:9-(4-Chlorobenzylidene)-2-nitro-9h-fluorene
CAS No.:4364-38-9
Molecular Formula:C₂₀H₁₂ClNO₂
Molecular Weight:333.774
Hs Code.:
European Community (EC) Number:654-355-7
Nikkaji Number:J978.408J
Mol file:4364-38-9.mol

Synonyms:9-(4-chlorobenzylidene)-2-nitro-9h-fluorene;4364-38-9

Suppliers and Price of 9-(4-Chlorobenzylidene)-2-nitro-9h-fluorene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
9-(4-CHLOROBENZYLIDENE)-2-NITROFLUORENE 95.00%
10G
$ 1183.57

American Custom Chemicals Corporation
9-(4-CHLOROBENZYLIDENE)-2-NITROFLUORENE 95.00%
5G
$ 844.91

American Custom Chemicals Corporation
9-(4-CHLOROBENZYLIDENE)-2-NITROFLUORENE 95.00%
1G
$ 628.51

Total 6 raw suppliers

Chemical Property of 9-(4-Chlorobenzylidene)-2-nitro-9h-fluorene

Chemical Property:

Vapor Pressure:3.33E-09mmHg at 25°C
Boiling Point:488.2°Cat760mmHg
Flash Point:249°C
PSA：45.82000
Density:1.391g/cm³
LogP:6.34070
XLogP3:5.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:333.0556563
Heavy Atom Count:24
Complexity:506

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

9-(4-CHLOROBENZYLIDENE)-2-NITROFLUORENE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=C(C2=CC4=CC=C(C=C4)Cl)C=C(C=C3)[N+](=O)[O-]
Isomeric SMILES:C1=CC=C\2C(=C1)C3=C(/C2=C\C4=CC=C(C=C4)Cl)C=C(C=C3)[N+](=O)[O-]

Technology Process of 9-(4-Chlorobenzylidene)-2-nitro-9h-fluorene

There total 4 articles about 9-(4-Chlorobenzylidene)-2-nitro-9h-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 607-57-8
2-nitro-9H-fluorene

: 104-88-1
4-chlorobenzaldehyde

: 136036-57-2,4364-38-9
9-(4-chloro-benzylidene)-2-nitro-fluorene

Guidance literature:: With di-(p-methoxyphenyl)tellurium oxide; In acetonitrile; for 1h; Ambient temperature; Irradiation;
DOI:10.1080/00397919708004087

Reference yield: 51.0%

: 607-57-8
2-nitro-9H-fluorene

: 104-88-1
4-chlorobenzaldehyde

: 4364-38-9
9-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-2-nitro-9H-fluorene

Guidance literature:: With potassium fluoride on basic alumina; In methanol; at 60 - 70 ℃; for 6h;
DOI:10.1080/00397910008087010

Reference yield:

: 607-57-8
2-nitro-9H-fluorene

: 104-88-1
4-chlorobenzaldehyde

: 136036-57-2,4364-38-9
9-(4-chloro-benzylidene)-2-nitro-fluorene

: 4364-38-9
9-[1-(4-Chloro-phenyl)-meth-(E)-ylidene]-2-nitro-9H-fluorene

Guidance literature:: With sodium hydroxide; butyltriethylammonium hydrogen sulfate; In tetrahydrofuran; at -4 ℃; for 3.5h; Title compound not separated from byproducts;
DOI:10.1002/(SICI)1097-458X(199807)36:7<520::AID-OMR327>3.0.CO;2-7