3-{[Dimethyl(phenyl)silyl]oxy}pentane-1,5-diol

Base Information

Chemical Name:3-{[Dimethyl(phenyl)silyl]oxy}pentane-1,5-diol
CAS No.:917387-26-9
Molecular Formula:C13H22O3Si
Molecular Weight:254.401
Hs Code.:
DSSTox Substance ID:DTXSID60580353
Nikkaji Number:J2.428.569C
Wikidata:Q82471172

Synonyms:917387-26-9;3-{[Dimethyl(phenyl)silyl]oxy}pentane-1,5-diol;DTXSID60580353;3-(dimethylphenylsilyloxy)pentane-1,5-diol

Suppliers and Price of 3-{[Dimethyl(phenyl)silyl]oxy}pentane-1,5-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 3-{[Dimethyl(phenyl)silyl]oxy}pentane-1,5-diol

Chemical Property:

Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:7
Exact Mass:254.13382109
Heavy Atom Count:17
Complexity:197

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[Si](C)(C1=CC=CC=C1)OC(CCO)CCO

Technology Process of 3-{[Dimethyl(phenyl)silyl]oxy}pentane-1,5-diol

There total 3 articles about 3-{[Dimethyl(phenyl)silyl]oxy}pentane-1,5-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 927403-88-1
dimethyl 3-(dimethylphenylsilyloxy)glutarate

: 917387-26-9
3-(dimethylphenylsilyloxy)pentane-1,5-diol

Guidance literature:: With lithium borohydride; In diethyl ether; at 20 ℃; for 17h;
DOI:10.1016/j.tetasy.2006.10.043

Reference yield:

: 7250-55-7
dimethyl 3-hydroxypentanedioate

: 917387-26-9
3-(dimethylphenylsilyloxy)pentane-1,5-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / imidazole / CH₂Cl₂ / 22 h / 20 °C

2: 85 percent / LiBH₄ / diethyl ether / 17 h / 20 °C

With 1H-imidazole; lithium borohydride; In diethyl ether; dichloromethane;
DOI:10.1016/j.tetasy.2006.10.043

Reference yield:

: 768-33-2
phenyldimethylsilyl chloride

: 917387-26-9
3-(dimethylphenylsilyloxy)pentane-1,5-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / imidazole / CH₂Cl₂ / 22 h / 20 °C

2: 85 percent / LiBH₄ / diethyl ether / 17 h / 20 °C

With 1H-imidazole; lithium borohydride; In diethyl ether; dichloromethane;
DOI:10.1016/j.tetasy.2006.10.043