Gold, (3,3-dimethyl-1-butynyl)(triphenylphosphine)-

Base Information

Chemical Name:Gold, (3,3-dimethyl-1-butynyl)(triphenylphosphine)-
CAS No.:91884-26-3
Molecular Formula:C24H24AuP
Molecular Weight:540.395
Hs Code.:

Synonyms:

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Chemical Property of Gold, (3,3-dimethyl-1-butynyl)(triphenylphosphine)-

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MSDS Files:: SDS file from LookChem

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Technology Process of Gold, (3,3-dimethyl-1-butynyl)(triphenylphosphine)-

There total 1 articles about Gold, (3,3-dimethyl-1-butynyl)(triphenylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 14243-64-2
(triphenylphosphine)gold(I) chloride

: 917-92-0
3,3-Dimethylbut-1-yne

: 91884-26-3
Au(-C*C-(t)Bu)(PPh₃)

Guidance literature:: copper(l) chloride; In diethylamine; under N2, 0.08 equiv of CuCl was added to stirred mixt. of Au-complex and ligand (molar ratio 1:1.02) in Et2NH, 30 min; solvent removed in vac. at room temp., water added, extd. with benzene,extract dried over MgSO4 overnight, evapd., washed with dry Et2O, recrystd. from toluene-n-octane; elem. anal.;

Reference yield: 85.0%

: 91884-26-3
Au(-C*C-(t)Bu)(PPh₃)

: 4648-54-8
trimethylsilylazide

: 922527-78-4
[(Ph₃P)Au(t-butyltriazole)]

Guidance literature:: With t-butylacetylene; In methanol; toluene; soln. of azide in toluene was added to soln. of Au complex in toluene; mixt. was stirred for 5 min; MeOH was added; stirred for 24 h; butylacetylene was added; stirred for 48 h; concd. (vac.); pentane added; cooled to -20°C; filtered; dried; elem. anal.;
DOI:10.1021/om0607200