2,6-dichloro-N,N-dimethylaniline

Base Information

Chemical Name:2,6-dichloro-N,N-dimethylaniline
CAS No.:56961-05-8
Molecular Formula:C8H9Cl2N
Molecular Weight:190.0698
Hs Code.:

Synonyms:

Suppliers and Price of 2,6-dichloro-N,N-dimethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,6-dichloro-N,N-dimethylaniline

Chemical Property:

Vapor Pressure:0.0912mmHg at 25°C
Boiling Point:224.4°Cat760mmHg
Flash Point:89.5°C
Density:1.256g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,6-dichloro-N,N-dimethylaniline

There total 9 articles about 2,6-dichloro-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 915144-99-9
4-bromo-2,6-dichloro-N,N-dimethylaniline

: 56961-05-8
N,N-Dimethyl-2,6-dichloroaniline

Guidance literature:: With hydrogen bromide; acetic acid; aniline; Reflux;
DOI:10.1021/acs.joc.9b02784

Reference yield: 25.0%

: 77-78-1
dimethyl sulfate

: 608-31-1
2,6-Dichloroaniline

: 56961-05-8
N,N-Dimethyl-2,6-dichloroaniline

Guidance literature:: dimethyl sulfate; 2,6-Dichloroaniline; With potassium carbonate; In toluene; Reflux;

With ammonia; In water; toluene; for 0.0833333h;
DOI:10.1515/znb-2012-0402

Reference yield:

: 62-53-3
aniline

: 56961-05-8
N,N-Dimethyl-2,6-dichloroaniline

Guidance literature:: Multi-step reaction with 3 steps

1: HCl(gas), Cl₂ / CCl₄; ethanol / ice-bath

2: 12 g / K₂CO₃ / toluene / Heating; overnight

3: NH₄HCO₂ / 10percent Pd/C / propan-2-ol / 1.5 h / Ambient temperature

With hydrogenchloride; ammonium formate; chlorine; potassium carbonate; palladium on activated charcoal; In tetrachloromethane; ethanol; isopropyl alcohol; toluene;
DOI:10.1016/S0040-4020(01)80400-2