3-(3-Bromopropyl)-2-methylcyclohex-2-en-1-one

Base Information

Chemical Name:3-(3-Bromopropyl)-2-methylcyclohex-2-en-1-one
CAS No.:91891-59-7
Molecular Formula:C₁₀H₁₅BrO
Molecular Weight:231.132
Hs Code.:
DSSTox Substance ID:DTXSID00533141
Wikidata:Q82406256

Synonyms:91891-59-7;3-(3-Bromopropyl)-2-methylcyclohex-2-en-1-one;DTXSID00533141

Suppliers and Price of 3-(3-Bromopropyl)-2-methylcyclohex-2-en-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(3-Bromopropyl)-2-methylcyclohex-2-en-1-one

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:230.03063
Heavy Atom Count:12
Complexity:206

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(CCCC1=O)CCCBr

Technology Process of 3-(3-Bromopropyl)-2-methylcyclohex-2-en-1-one

There total 4 articles about 3-(3-Bromopropyl)-2-methylcyclohex-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100466-71-5
3-(3-((methanesulfonyl)oxy)propyl)-2-methyl-2-cyclohexenone

: 91891-59-7
3-(3-bromopropyl)-2-methyl-2-cyclohexenone

Guidance literature:: With lithium bromide; In tetrahydrofuran; for 15h; Ambient temperature;
DOI:10.1021/jo00359a019

Reference yield:

: 20643-20-3
3-ethoxy-2-methyl-2-cyclohexen-1-one

: 91891-59-7
3-(3-bromopropyl)-2-methyl-2-cyclohexenone

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) Mg, dibromoethane / 1.) THF, RT, 2 h, 2.) THF, RT, 15 h

2: 0.738 g / oxalic acid / methanol / 6 h / Ambient temperature

3: 1.068 g / Et₃N / tetrahydrofuran / 2 h / Ambient temperature

4: 997 mg / LiBr / tetrahydrofuran / 15 h / Ambient temperature

With 1,1-Dibromoethane; oxalic acid; magnesium; triethylamine; lithium bromide; In tetrahydrofuran; methanol;
DOI:10.1021/jo00359a019

Reference yield:

: 100466-70-4
3-(3-hydroxypropyl)-2-methyl-2-cyclohexenone

: 91891-59-7
3-(3-bromopropyl)-2-methyl-2-cyclohexenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1.068 g / Et₃N / tetrahydrofuran / 2 h / Ambient temperature

2: 997 mg / LiBr / tetrahydrofuran / 15 h / Ambient temperature

With triethylamine; lithium bromide; In tetrahydrofuran;
DOI:10.1021/jo00359a019