Boranetriamine, [2,4,6-tris(1,1-dimethylethyl)phenyl]-

Base Information

Chemical Name:Boranetriamine, [2,4,6-tris(1,1-dimethylethyl)phenyl]-
CAS No.:91915-29-6
Molecular Formula:C₁₈H₃₄BN₃
Molecular Weight:303.299
Hs Code.:

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Chemical Property of Boranetriamine, [2,4,6-tris(1,1-dimethylethyl)phenyl]-

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Technology Process of Boranetriamine, [2,4,6-tris(1,1-dimethylethyl)phenyl]-

There total 2 articles about Boranetriamine, [2,4,6-tris(1,1-dimethylethyl)phenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 91915-27-4
BCl₂(NHC₆H₂But₃-2,4,6)

: 91915-29-6
B(NH₂)2(NHC₆H₂But₃-2,4,6)

Guidance literature:: With NH₃; In hexane; react. BCl2(NHC6H2But3-2,4,6) with excess NH3(g) in n-C6H14 at 25°C for 3 h; filtration and crystn. at -30°C from concd. filtrate followed bysublimation; elem. anal.;
DOI:10.1039/c39840000662

Reference yield:

: 102745-24-4
2,4,6-tri-t-butylanilidolithium

: 91915-29-6
B(NH₂)2(NHC₆H₂But₃-2,4,6)

Guidance literature:: Multi-step reaction with 2 steps

1: hexane

2: NH₃ / hexane

With NH₃; In hexane;
DOI:10.1039/c39840000662

Reference yield: 56.0%

: tetrafluoroboric acid

: 91915-29-6
B(NH₂)2(NHC₆H₂But₃-2,4,6)

: 91915-30-9
(NH₃C₆H₂But₃-2,4,6)(BF₄)

Guidance literature:: In diethyl ether; react. B(NH2)2(NHC6H2But3-2,4,6) with 10-fold excess H(BF4) in OEt2 at 25°C for 12 h; elem. anal.;
DOI:10.1039/c39840000662