4-(2-BROMOPHENYL)BUTANOYL CHLORIDE

Base Information

Chemical Name:4-(2-BROMOPHENYL)BUTANOYL CHLORIDE
CAS No.:92013-30-4
Molecular Formula:C₁₀H₁₀BrClO
Molecular Weight:261.546
Hs Code.:
Mol file:92013-30-4.mol

Synonyms:

Suppliers and Price of 4-(2-BROMOPHENYL)BUTANOYL CHLORIDE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 4-(2-BROMOPHENYL)BUTANOYL CHLORIDE

Chemical Property:

PSA：17.07000
LogP:3.53720

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(2-BROMOPHENYL)BUTANOYL CHLORIDE

There total 11 articles about 4-(2-BROMOPHENYL)BUTANOYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3433-80-5
1-Bromo-2-bromomethyl-benzene

: 92013-30-4
4-(o-bromophenyl)butyryl chloride

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / tetrahydrofuran; diethyl ether / 1.5 h / Heating

2: 73 percent / 9-BBN, 6M NaOH, 30percent H₂O₂ / 1.5 h / 50 °C

3: 66 percent / chromium trioxide, 1.5M sulfuric acid / acetone / 4 h / 0 °C

4: thionyl chloride / 2.5 h / Ambient temperature

With chromium(VI) oxide; sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; thionyl chloride; sulfuric acid; dihydrogen peroxide; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1016/0040-4020(96)00266-9

Reference yield:

: 123206-83-7
4-(2-Bromophenyl)-1-butanol

: 92013-30-4
4-(o-bromophenyl)butyryl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / chromium trioxide; acetic acid / 18 h / 20 °C

2: thionyl chloride / 0.75 h / Heating

With chromium(VI) oxide; thionyl chloride; acetic acid;
DOI:10.1016/j.bmc.2006.05.077

Reference yield:

: 71813-50-8
1-bromo-2-(but-3-enyl)benzene

: 92013-30-4
4-(o-bromophenyl)butyryl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: 9-borabicyclo[3.3.1]nonane / hexane / 18 h / 20 °C

1.2: 82 percent / NaOH; H₂O₂ / tetrahydrofuran / 1.5 h / 50 °C

2.1: 58 percent / chromium trioxide; acetic acid / 18 h / 20 °C

3.1: thionyl chloride / 0.75 h / Heating

With chromium(VI) oxide; thionyl chloride; acetic acid; 9-bora-bicyclo[3.3.1]nonane; In hexane;
DOI:10.1016/j.bmc.2006.05.077