Technology Process of Benzoic acid, 3-amino-5-[2-(1,1-dimethylethoxy)-2-oxoethoxy]-, methyl
ester
There total 5 articles about Benzoic acid, 3-amino-5-[2-(1,1-dimethylethoxy)-2-oxoethoxy]-, methyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
for 18h;
under 1810.02 Torr;
DOI:10.1021/jm00378a005
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) aq. H2SO4, NaN2, 2.) aq H2SO4 / 2.) reflux, 30 min
2: 82.4 percent / AcCl / 18 h / Ambient temperature
3: 81 percent / NaH / tetrahydrofuran / 8 h / Heating
4: 86 percent / H2 / 10percent Pd/C / methanol / 18 h / 1810.02 Torr
With
sulfuric acid; hydrogen; sodium hydride; acetyl chloride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol;
DOI:10.1021/jm00378a005
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 80 percent / 1.) aq. NH3, 2.) H2S
2: 1.) aq. H2SO4, NaN2, 2.) aq H2SO4 / 2.) reflux, 30 min
3: 82.4 percent / AcCl / 18 h / Ambient temperature
4: 81 percent / NaH / tetrahydrofuran / 8 h / Heating
5: 86 percent / H2 / 10percent Pd/C / methanol / 18 h / 1810.02 Torr
With
ammonium hydroxide; sulfuric acid; hydrogen sulfide; hydrogen; sodium hydride; acetyl chloride;
palladium on activated charcoal;
In
tetrahydrofuran; methanol;
DOI:10.1021/jm00378a005
