Technology Process of Benzenepropanoic acid, 3-amino-a-hydroxy-
There total 4 articles about Benzenepropanoic acid, 3-amino-a-hydroxy- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
5%-palladium/activated carbon;
In
methanol;
for 1h;
under 517.162 Torr;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: acetic anhydride; sodium acetate / 6 h / 120 °C
2.1: hydrogenchloride; water / 6 h / 100 °C
3.1: sodium ethanolate / methanol / 0 °C
3.2: 0.5 h / 5 - 10 °C
4.1: 5%-palladium/activated carbon; hydrogen / methanol / 1 h / 517.16 Torr
With
hydrogenchloride; 5%-palladium/activated carbon; water; hydrogen; sodium ethanolate; sodium acetate; acetic anhydride;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium ethanolate / methanol / 0 °C
1.2: 0.5 h / 5 - 10 °C
2.1: 5%-palladium/activated carbon; hydrogen / methanol / 1 h / 517.16 Torr
With
5%-palladium/activated carbon; hydrogen; sodium ethanolate;
In
methanol;