3-Pentanone, 2-(3,4-dimethoxyphenyl)-

Base Information

Chemical Name:3-Pentanone, 2-(3,4-dimethoxyphenyl)-
CAS No.:92156-84-8
Molecular Formula:C13H18O3
Molecular Weight:222.284
Hs Code.:2914509090

Synonyms:Oxirane,(3,4-dimethoxyphenyl);2-(3',4'-dimethoxyphenyl)-oxirane;2-(3,4-dimethoxyphenyl)pentan-3-one;3,4-dimethoxystyrene oxide;

Suppliers and Price of 3-Pentanone, 2-(3,4-dimethoxyphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2-(3,4-Dimethoxyphenyl)pentan-3-one 95+%
1g
$ 402.00

Alichem
2-(3,4-Dimethoxyphenyl)pentan-3-one
1g
$ 321.44

Total 4 raw suppliers

Chemical Property of 3-Pentanone, 2-(3,4-dimethoxyphenyl)-

Chemical Property:

Boiling Point:308.0±37.0 °C(Predicted)
PSA：35.53000
Density:1.021±0.06 g/cm3(Predicted)
LogP:2.78640

Purity/Quality:

≥99% ^*data from raw suppliers

2-(3,4-Dimethoxyphenyl)pentan-3-one 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Pentanone, 2-(3,4-dimethoxyphenyl)-

There total 4 articles about 3-Pentanone, 2-(3,4-dimethoxyphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 925-90-6
ethylmagnesium bromide

: 193412-02-1
N-methyl-N-methoxy-2-(3',4'-dimethoxyphenyl)propanamide

: 92156-84-8
2-(3,4-dimethoxyphenyl)pentan-3-one

Guidance literature:: In tetrahydrofuran; diethyl ether; 1.) 0 deg C, 1 h, 2.) room temperature, 1 h;
DOI:10.1021/jo970570q

Reference yield: 77.0%

: 2859-78-1
4-Bromoveratrole

: 96-22-0
pentan-3-one

: 92156-84-8
2-(3,4-dimethoxyphenyl)pentan-3-one

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; sodium t-butanolate; 1,3,5,7-tetramethyl-8-phenyl-2,4,6-trioxa-8-phosphatricyclo[3.3.1.13,7]decane; In toluene; at 40 ℃; for 20h; Inert atmosphere;
DOI:10.1021/ol202565j

Reference yield:

: 93-40-3
(3,4-Dimethoxyphenyl)acetic acid

: 92156-84-8
2-(3,4-dimethoxyphenyl)pentan-3-one

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / LDA / tetrahydrofuran / 1.) -78 deg C, 1 h, 2.) room temperature, 4 h

2: 1.) oxalyl chloride, 2.) pyridine / 1.) benzene, room temperature, 17 h, 2.) CH₂Cl₂, room temperature, 2 h

3: 93 percent / tetrahydrofuran; diethyl ether / 1.) 0 deg C, 1 h, 2.) room temperature, 1 h

With pyridine; oxalyl dichloride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo970570q