2-Naphthalenecarboxylic acid, 4-hydroxy-5-methoxy-, ethyl ester

Base Information

Chemical Name:2-Naphthalenecarboxylic acid, 4-hydroxy-5-methoxy-, ethyl ester
CAS No.:92191-07-6
Molecular Formula:C14H14O4
Molecular Weight:
Hs Code.:
DSSTox Substance ID:DTXSID30443466
Wikidata:Q82261309

Synonyms:92191-07-6;2-Naphthalenecarboxylic acid, 4-hydroxy-5-methoxy-, ethyl ester;2-Naphthalenecarboxylic acid,4-hydroxy-5-methoxy-,ethyl ester;Ethyl 4-hydroxy-5-methoxynaphthalene-2-carboxylate;DTXSID30443466

Suppliers and Price of 2-Naphthalenecarboxylic acid, 4-hydroxy-5-methoxy-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Naphthalenecarboxylic acid, 4-hydroxy-5-methoxy-, ethyl ester

Chemical Property:

Vapor Pressure:0mmHg at 25°C
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:246.08920892
Heavy Atom Count:18
Complexity:292

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C1=CC(=C2C(=C1)C=CC=C2OC)O

Technology Process of 2-Naphthalenecarboxylic acid, 4-hydroxy-5-methoxy-, ethyl ester

There total 8 articles about 2-Naphthalenecarboxylic acid, 4-hydroxy-5-methoxy-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: ethyl 8-bromo-4-hydroxy-5-methoxy-2-naphthoate

: 92191-07-6
ethyl 4-hydroxy-5-methoxy-2-naphthoate

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; at 35 ℃; for 12h; Sealed tube; Inert atmosphere;
DOI:10.1002/chem.201903832

Reference yield: 90.0%

: 72586-64-2
ethyl 4-acetoxy-8-bromo-5-methoxy-2-naphthoate

: 92191-07-6
ethyl 4-hydroxy-5-methoxy-2-naphthoate

Guidance literature:: ethyl 4-acetoxy-8-bromo-5-methoxy-2-naphthoate; With palladium 10% on activated carbon; hydrogen; In ethanol; dichloromethane; at 25 ℃; for 48h;

With sodium ethanolate; at 0 - 25 ℃; for 24h; Inert atmosphere;
DOI:10.1055/s-0036-1589118

Reference yield:

: 31129-14-3
3-Ethoxycarbonyl-4-(m-methoxyphenyl)-3-butensaeure

: 92191-07-6
ethyl 4-hydroxy-5-methoxy-2-naphthoate

: 173483-53-9
ethyl 1-hydroxy-6-methoxynaphthalene-3-carboxylate

Guidance literature:: With sodium acetate; acetic anhydride; potassium carbonate; Yield given. Multistep reaction. Yields of byproduct given; 1.) 70 deg C, 10 h, 2.) EtOH, reflux, 4 h;
DOI:10.1021/jo952033g