9,11-Dioxa-2-aza-10-phosphatridecanoic acid, 10-[bis(1-methylethyl)amino]-13-cyano-, 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl ester

Base Information

Chemical Name:9,11-Dioxa-2-aza-10-phosphatridecanoic acid, 10-[bis(1-methylethyl)amino]-13-cyano-, 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl ester
CAS No.:922522-12-1
Molecular Formula:C38H53N4O5P
Molecular Weight:676.836
Hs Code.:

9,11-Dioxa-2-aza-10-phosphatridecanoic acid,
10-[bis(1-methylethyl)amino]-13-cyano-,
2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl ester

Synonyms:1-N-[2-(4-monomethoxytrityl)aminoethoxycarbonyl]amino-6-hexanol 6-O-(2-cyanoethyl-N,N-diisopropylphosphoramidite);1-N-[2-(4'-monomethoxytrityl)aminoethoxycarbonyl]amino-6-hexanol 6-O-(2-cyanoethyl-N,N-diisopropylphosphoramidite);

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9,11-Dioxa-2-aza-10-phosphatridecanoic acid, 10-[bis(1-methylethyl)amino]-13-cyano-, 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl ester

Chemical Property:

Boiling Point:723.8±60.0 °C(Predicted)
PSA：118.67000
LogP:8.93768

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9,11-Dioxa-2-aza-10-phosphatridecanoic acid, 10-[bis(1-methylethyl)amino]-13-cyano-, 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl ester

There total 1 articles about 9,11-Dioxa-2-aza-10-phosphatridecanoic acid, 10-[bis(1-methylethyl)amino]-13-cyano-, 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 922522-11-0
1-N-[2'-(4-monomethoxytrityl)aminoethoxycarbonyl]amino-6-hexanol

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 922522-12-1
1-N-[2'-(4-monomethoxytrityl)aminoethoxycarbonyl]amino-6-hexanol 6-O-(2-cyanoethyl-N,N-diisopropylphosphoramidite)

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1016/j.bmc.2007.10.011

Reference yield:

: 922522-12-1
1-N-[2'-(4-monomethoxytrityl)aminoethoxycarbonyl]amino-6-hexanol 6-O-(2-cyanoethyl-N,N-diisopropylphosphoramidite)

: 98796-51-1
5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-[O-(2-cyanoethyl)-N,N'-diisopropylphosphoramidite]

: 112667-29-5
N-(9-fluorenylmethoxycarbonyl)-L-phenylalaninamide

: 64-19-7,77671-22-8
acetic acid

: 1017241-12-1
5'-[6-((2-aminoethoxy)carbonyl)aminohexyl]-TTTTT-3'

: 5'-[6-((2-acetylaminoethoxy)carbonyl)aminohexyl]-TTTTT-3'

: 1159182-97-4
Phe-ssH-T₅

Guidance literature:: 5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-[O-(2-cyanoethyl)-N,N'-diisopropylphosphoramidite]; Automated synthesizer; solid phase reaction;

5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-[O-(2-cyanoethyl)-N,N'-diisopropylphosphoramidite]; Automated synthesizer; solid phase reaction;

1-N-[2'-(4-monomethoxytrityl)aminoethoxycarbonyl]amino-6-hexanol 6-O-(2-cyanoethyl-N,N-diisopropylphosphoramidite); 5'-O-(4,4'-dimethoxytrityl)-2'-deoxythymidine-3'-O-[O-(2-cyanoethyl)-N,N'-diisopropylphosphoramidite]; N-(9-fluorenylmethoxycarbonyl)-L-phenylalaninamide; acetic acid; Further stages;
DOI:10.1016/j.bmcl.2009.02.121