Technology Process of 1-((2-Hydroxy-1-(hydroxymethyl)ethoxy)methyl)-5-benzyluracil
There total 3 articles about 1-((2-Hydroxy-1-(hydroxymethyl)ethoxy)methyl)-5-benzyluracil which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene / a) RT, 24 h, b) reflux, 24 h
2: 67 percent / H2 / 10percent Pd/C / methanol / 18 h / 2327.2 Torr / Ambient temperature
With
hydrogen;
palladium on activated charcoal;
In
methanol; toluene;
DOI:10.1021/jm00145a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: ammonium sulfate / 12 h / Heating
2: toluene / a) RT, 24 h, b) reflux, 24 h
3: 67 percent / H2 / 10percent Pd/C / methanol / 18 h / 2327.2 Torr / Ambient temperature
With
ammonium sulfate; hydrogen;
palladium on activated charcoal;
In
methanol; toluene;
DOI:10.1021/jm00145a023
