Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine, 6-chloro-

Base Information

Chemical Name:Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine, 6-chloro-
CAS No.:87213-32-9
Molecular Formula:C₁₄H₈ClN₃S
Molecular Weight:285.757
Hs Code.:
DSSTox Substance ID:DTXSID80236188
Wikidata:Q83118108

Synonyms:BRN 4491511;Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine, 6-chloro-;6-Chlorodibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine;8-Chloro-(1,2,4)-triazolo(4,3-d)(b,e)-1,4-dibenzothiazepine;87213-32-9;C14H8ClN3S;C14-H8-Cl-N3-S;DTXSID80236188;LS-61515

Suppliers and Price of Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine, 6-chloro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine, 6-chloro-

Chemical Property:

Vapor Pressure:1.27E-11mmHg at 25°C
Boiling Point:537.4°C at 760 mmHg
Flash Point:278.8°C
Density:1.52g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:285.0127461
Heavy Atom Count:19
Complexity:343

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C3=NN=CN3C4=C(S2)C=CC(=C4)Cl

Technology Process of Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine, 6-chloro-

There total 9 articles about Dibenzo(b,f)-1,2,4-triazolo(4,3-d)(1,4)thiazepine, 6-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 87213-29-4
8-chloro-11-hydrazinodibenzo-1,4-thiazepine

: 122-51-0
orthoformic acid triethyl ester

: 87213-32-9
6-chlorodibenzo-1,2,4-triazolo<4,3-d>-1,4-thiazepine

Guidance literature:: With sulfuric acid; In ethanol; for 1.5h;
DOI:10.1135/cccc19831465

Reference yield:

: 122032-99-9
8-amino-11-chloro-10,11-dihydro-dibenzo<1,4>thiazepine

: 87213-32-9
6-chlorodibenzo-1,2,4-triazolo<4,3-d>-1,4-thiazepine

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / NH₂NH₂*H₂O / glycerol / 6 h / Heating

2: 60 percent / dioxane / 4 h / Heating

4: HClO₄ / CuCl

With perchloric acid; hydrazine hydrate; copper(l) chloride; In 1,4-dioxane; glycerol;

Reference yield:

: 105554-89-0
8-amino-10,11-dihydro-dibenzo<1,4>thiazepin-11-one

: 87213-32-9
6-chlorodibenzo-1,2,4-triazolo<4,3-d>-1,4-thiazepine

Guidance literature:: Multi-step reaction with 5 steps

1: 70 percent / HCl gas / POCl₃ / 1.5 h / Heating

2: 68 percent / NH₂NH₂*H₂O / glycerol / 6 h / Heating

3: 60 percent / dioxane / 4 h / Heating

5: HClO₄ / CuCl

With hydrogenchloride; perchloric acid; hydrazine hydrate; copper(l) chloride; In 1,4-dioxane; glycerol; trichlorophosphate;