Benzene, 1-chloro-3-fluoro-2,4,5,6-tetranitro-

Base Information

Chemical Name:Benzene, 1-chloro-3-fluoro-2,4,5,6-tetranitro-
CAS No.:92367-10-7
Molecular Formula:C6ClFN4O8
Molecular Weight:310.539
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 1-chloro-3-fluoro-2,4,5,6-tetranitro-

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Technology Process of Benzene, 1-chloro-3-fluoro-2,4,5,6-tetranitro-

There total 5 articles about Benzene, 1-chloro-3-fluoro-2,4,5,6-tetranitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73333-99-0
Pentanitrofluorobenzene

: 92367-10-7
3-chloro-2,4,5,6-tetranitrofluorobenzene

Guidance literature:: With hydrogenchloride; In benzene; at 25 ℃; for 2h; Yield given;
DOI:10.1021/jo00198a001

Reference yield:

: 2365-71-1
3,5-dinitro-4-fluorobenzoic acid

: 92367-10-7
3-chloro-2,4,5,6-tetranitrofluorobenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 20percent oleum, NaN₃ / 1,2-dichloro-ethane / 1 h / Heating

2: 90percent HNO₃ / aq. H₂SO₄ / 4.5 h / 20 - 30 °C

3: anisole / aq. H₂SO₄ / 1 h / 25 °C

4: 98percent H₂O₂, 20percent oleum / 16 h / 25 °C

5: conc. HCl / benzene / 2 h / 25 °C

With hydrogenchloride; sodium azide; sulfuric acid; dihydrogen peroxide; nitric acid; methoxybenzene; In sulfuric acid; 1,2-dichloro-ethane; benzene;
DOI:10.1021/jo00198a001

Reference yield:

: 92367-07-2
3,5-dinitro-4-fluoro aniline

: 92367-10-7
3-chloro-2,4,5,6-tetranitrofluorobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 90percent HNO₃ / aq. H₂SO₄ / 4.5 h / 20 - 30 °C

2: anisole / aq. H₂SO₄ / 1 h / 25 °C

3: 98percent H₂O₂, 20percent oleum / 16 h / 25 °C

4: conc. HCl / benzene / 2 h / 25 °C

With hydrogenchloride; sulfuric acid; dihydrogen peroxide; nitric acid; methoxybenzene; In sulfuric acid; benzene;
DOI:10.1021/jo00198a001