2,6,10,14,18,22,26,30,34-Hexatriacontanonaen-1-ol, 3,7,11,15,19,23,27,31,35-nonamethyl-, dihydrogen phosphate, diammonium salt, (Z,Z,Z,Z,Z,Z,E,E)-

Base Information

Chemical Name:2,6,10,14,18,22,26,30,34-Hexatriacontanonaen-1-ol, 3,7,11,15,19,23,27,31,35-nonamethyl-, dihydrogen phosphate, diammonium salt, (Z,Z,Z,Z,Z,Z,E,E)-
CAS No.:92466-33-6
Molecular Formula:C45H75O4P.2H3N
Molecular Weight:
Hs Code.:

2,6,10,14,18,22,26,30,34-Hexatriacontanonaen-1-ol,
3,7,11,15,19,23,27,31,35-nonamethyl-, dihydrogen phosphate,
diammonium salt, (Z,Z,Z,Z,Z,Z,E,E)-

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Chemical Property of 2,6,10,14,18,22,26,30,34-Hexatriacontanonaen-1-ol, 3,7,11,15,19,23,27,31,35-nonamethyl-, dihydrogen phosphate, diammonium salt, (Z,Z,Z,Z,Z,Z,E,E)-

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Technology Process of 2,6,10,14,18,22,26,30,34-Hexatriacontanonaen-1-ol, 3,7,11,15,19,23,27,31,35-nonamethyl-, dihydrogen phosphate, diammonium salt, (Z,Z,Z,Z,Z,Z,E,E)-

There total 5 articles about 2,6,10,14,18,22,26,30,34-Hexatriacontanonaen-1-ol, 3,7,11,15,19,23,27,31,35-nonamethyl-, dihydrogen phosphate, diammonium salt, (Z,Z,Z,Z,Z,Z,E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Phosphoric acid bis-(2-cyano-ethyl) ester (2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethyl-hexatriaconta-2,6,10,14,18,22,26,30,34-nonaenyl ester

: 92466-33-6,99531-13-2,128715-80-0
Phosphoric acid mono-((2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethyl-hexatriaconta-2,6,10,14,18,22,26,30,34-nonaenyl) ester; compound with ammonia

Guidance literature:: Phosphoric acid bis-(2-cyano-ethyl) ester (2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethyl-hexatriaconta-2,6,10,14,18,22,26,30,34-nonaenyl ester; With methanol; sodium methylate; at 20 ℃; for 24h;

In methanol; Further stages;
DOI:10.1002/ejoc.201301089

Reference yield:

: 2,2,2-Trichloro-acetimidic acid (2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethyl-hexatriaconta-2,6,10,14,18,22,26,30,34-nonaenyl ester

: 92466-33-6,99531-13-2,128715-80-0
Phosphoric acid mono-((2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethyl-hexatriaconta-2,6,10,14,18,22,26,30,34-nonaenyl) ester; compound with ammonia

: 92466-34-7
Phosphoric acid mono-((4E,8E,12E,16E,20E,24E,28E)-1,5,9,13,17,21,25,29,33-nonamethyl-1-vinyl-tetratriaconta-4,8,12,16,20,24,28,32-octaenyl) ester; compound with ammonia

Guidance literature:: With phosphoric acid; In tetrahydrofuran; at 20 ℃; for 0.25h; Yield given. Yields of byproduct given;
DOI:10.1055/s-1984-30853

Reference yield:

: 13190-97-1,540-03-4
solanesol

: 92466-33-6,99531-13-2,128715-80-0
Phosphoric acid mono-((2E,6E,10E,14E,18E,22E,26E,30E)-3,7,11,15,19,23,27,31,35-nonamethyl-hexatriaconta-2,6,10,14,18,22,26,30,34-nonaenyl) ester; compound with ammonia

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-tetrazole / tetrahydrofuran / 0 - 20 °C

2.1: sodium periodate; pyridine / tetrahydrofuran / 0 - 20 °C

3.1: sodium methylate; methanol / 24 h / 20 °C

3.2: Amberlyst-15

With pyridine; 1H-tetrazole; methanol; sodium periodate; sodium methylate; In tetrahydrofuran;
DOI:10.1002/ejoc.201301089