Tetrabutylammonium hydrogen sulfide

Base Information

Chemical Name:Tetrabutylammonium hydrogen sulfide
CAS No.:84030-21-7
Molecular Formula:C₁₆H₃₆N*HS
Molecular Weight:275.542
Hs Code.:
European Community (EC) Number:281-792-7
Mol file:84030-21-7.mol

Synonyms:Tetrabutylammonium hydrogen sulfide;84030-21-7;sulfanide;tetrabutylazanium;Tetrabutylammonium hydrogen sulphide;EINECS 281-792-7;C16H36N.HS;SCHEMBL2007036;tetrabutylammonium hydrogensulfide;C16-H36-N.H-S;FT-0674938;1-Butanaminium, N,N,N-tributyl-, sulfide (1:1)

Suppliers and Price of Tetrabutylammonium hydrogen sulfide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
TetrabutylammoniumHydrogenSulfide
50g
$ 3300.00

American Custom Chemicals Corporation
TETRABUTYLAMMONIUM HYDROGEN SULFIDE 95.00%
50G
$ 5775.00

Total 7 raw suppliers

Chemical Property of Tetrabutylammonium hydrogen sulfide

Chemical Property:

PSA：38.80000
LogP:4.73350
Storage Temp.:2-8°C
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:12
Exact Mass:275.26467136
Heavy Atom Count:18
Complexity:116

Purity/Quality:

98%Min ^*data from raw suppliers

TetrabutylammoniumHydrogenSulfide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi
Statements: 36/38
Safety Statements: 26-36

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[N+](CCCC)(CCCC)CCCC.[SH-]
Uses A convenient reagent for thiolation of 1,1-dichloroalkenes.

Technology Process of Tetrabutylammonium hydrogen sulfide

There total 1 articles about Tetrabutylammonium hydrogen sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: sodium hydrogen sulfide

: 1112-67-0
tetrabutyl-ammonium chloride

: 84030-21-7
tetrabutylammonium hydrogen sulfide

Guidance literature:: In acetonitrile; for 72h; Inert atmosphere;
DOI:10.1039/c5dt03355a

Reference yield: 51.0%

: 84030-21-7
tetrabutylammonium hydrogen sulfide

: 494843-61-7
[PhB(CH₂PPh₂)₃]FeCl

: ([PhBP₃]Fe)₂(μ-S)

Guidance literature:: With triethylamine; In tetrahydrofuran; benzene; at 20 ℃; for 2.08333h; Inert atmosphere;
DOI:10.1002/anie.201401018

Reference yield:

: 84030-21-7
tetrabutylammonium hydrogen sulfide

: 109309-12-8
MoO₂{N,N'-dimethyl-N,N'-bis(2-mercaptophenyl)ethylenediamine}

: 2001-45-8
tetraphenyl phosphonium chloride

: (Ph₄P){MoOS(N,N'.dimethyl-N,N'-bis(2-mercaptophenyl)ethylenediamine)}

Guidance literature:: In tetrahydrofuran; MoO2(C16H18N2S2) and (n-Bu4N)SH in THF stirred for 3 h, Ph4Cl added and stirred for 3 h; reducing volume, addition of water, filtration, washing with EtOH, recrystallization from THF/hexane, identification: elem. anal., IR, UV;