2-methoxy-7H-benzo[de]anthracen-7-one

Base Information

• Chemical Name: 2-methoxy-7H-benzo[de]anthracen-7-one
• CAS No.: 6535-67-7
• Molecular Formula: C18H12 O2
• Molecular Weight: 260.292
• Mol file: 6535-67-7.mol

Synonyms:2-Methoxybenzanthrone

Chemical Property of 2-methoxy-7H-benzo[de]anthracen-7-one

Chemical Property:

• Vapor Pressure: 5.95E-09mmHg at 25°C
• Boiling Point: 468.5°C at 760 mmHg
• Flash Point: 224.7°C
• PSA: 26.30000
• Density: 1.282g/cm³
• LogP: 4.05980

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-methoxy-7H-benzo[de]anthracen-7-one

There total 11 articles about 2-methoxy-7H-benzo[de]anthracen-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-hydroksybenzanthrone (61994-44-3) + dimethyl sulfate (77-78-1) → 2-methoxy-benz[de]anthracen-7-one (6535-67-7)

Guidance literature:

With aqueous alkali;

Reference yield:

3-aminobenzanthrone (13456-80-9) → 2-methoxy-benz[de]anthracen-7-one (6535-67-7)

Guidance literature:

Multi-step reaction with 5 steps

2: acetic acid; nitric acid

3: ethanolic sulfuric acid

4: concentrated sulfuric acid; NaNO₂ / Eintragen von Eis in das Reaktionsgemisch und Erwaermen des Reaktionsprodukts mit Aluminium-Pulver und Aethanol

5: aqueous NaOH

With sodium hydroxide; sulfuric acid; nitric acid; acetic acid; sodium nitrite;

DOI:10.1039/jr9480001088

Reference yield:

3-acetylaminobenzanthrone (53652-25-8) → 2-methoxy-benz[de]anthracen-7-one (6535-67-7)

Guidance literature:

Multi-step reaction with 4 steps

1: acetic acid; nitric acid

2: ethanolic sulfuric acid

3: concentrated sulfuric acid; NaNO₂ / Eintragen von Eis in das Reaktionsgemisch und Erwaermen des Reaktionsprodukts mit Aluminium-Pulver und Aethanol

4: aqueous NaOH

With sodium hydroxide; sulfuric acid; nitric acid; acetic acid; sodium nitrite;

DOI:10.1039/jr9480001088

upstream raw materials:

2-(3-methoxy-[1]naphthyl)-benzoic acid

2-hydroksybenzanthrone

dimethyl sulfate

benzene

Downstream raw materials:

Jade Green XBN