Technology Process of 4-Methylsalicylic acid
There total 66 articles about 4-Methylsalicylic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-chloro-4-methylbenzoic acid;
With
calcium hydroxide; water;
at 85 ℃;
for 1h;
With
water;
trans-N,N'-dimethyl-1,2-cyclohexyldiamine; copper(I) bromide;
at 80 ℃;
for 24h;
With
hydrogenchloride;
In
water;
at 25 ℃;
Product distribution / selectivity;
- Guidance literature:
-
With
oxygen; potassium acetate; palladium diacetate; p-benzoquinone;
In
N,N-dimethyl acetamide;
at 115 ℃;
for 15h;
under 760.051 Torr;
DOI:10.1021/ja907198n
- Guidance literature:
-
With
carbon dioxide;
at 185 ℃;
for 7h;
under 7600.51 Torr;
regioselective reaction;
Autoclave;
DOI:10.1134/S0965544116070161
Xn, 
Xi
