Benzenamine, 4-(3-fluoropropyl)-3-(trifluoromethyl)-

Base Information

Chemical Name:Benzenamine, 4-(3-fluoropropyl)-3-(trifluoromethyl)-
CAS No.:924909-37-5
Molecular Formula:C10H11F4N
Molecular Weight:221.198
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenamine, 4-(3-fluoropropyl)-3-(trifluoromethyl)-

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Technology Process of Benzenamine, 4-(3-fluoropropyl)-3-(trifluoromethyl)-

There total 4 articles about Benzenamine, 4-(3-fluoropropyl)-3-(trifluoromethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 924909-36-4
1-(3-fluoropropyl)-4-nitro-2-(trifluoromethyl)benzene

: 924909-37-5
4-(3-fluoropropyl)-3-(trifluoromethyl)aniline

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; at 20 ℃; for 3h;

Reference yield:

: 924909-34-2
3-(4-nitro-2-(trifluoromethyl)phenyl)-propionaldehyde

: 924909-37-5
4-(3-fluoropropyl)-3-(trifluoromethyl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1: methanol; sodium tetrahydroborate / 1 h / 20 °C

2: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 0 °C

3: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 20 °C

With methanol; sodium tetrahydroborate; diethylamino-sulfur trifluoride; hydrogen; palladium 10% on activated carbon; In methanol; dichloromethane;

Reference yield:

: 367-67-9
2-bromo-5-nitro-benzotrifluoride

: 924909-37-5
4-(3-fluoropropyl)-3-(trifluoromethyl)aniline

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutyl-ammonium chloride; triethylamine / palladium diacetate / N,N-dimethyl-formamide / 0.5 h / 90 °C

2: methanol; sodium tetrahydroborate / 1 h / 20 °C

3: diethylamino-sulfur trifluoride / dichloromethane / 1 h / 0 °C

4: hydrogen / palladium 10% on activated carbon / methanol / 3 h / 20 °C

With methanol; sodium tetrahydroborate; diethylamino-sulfur trifluoride; tetrabutyl-ammonium chloride; hydrogen; triethylamine; palladium diacetate; palladium 10% on activated carbon; In methanol; dichloromethane; N,N-dimethyl-formamide;