2(5H)-Furanone, 4-[2-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)ethenyl]-5-(2-oxoprop ylidene)-, (Z,E)-

Base Information

Chemical Name:2(5H)-Furanone, 4-[2-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)ethenyl]-5-(2-oxoprop ylidene)-, (Z,E)-
CAS No.:92510-15-1
Molecular Formula:C₁₉H₂₄O₄
Molecular Weight:316.397
Hs Code.:

Synonyms:

Suppliers and Price of 2(5H)-Furanone, 4-[2-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)ethenyl]-5-(2-oxoprop ylidene)-, (Z,E)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2(5H)-Furanone, 4-[2-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)ethenyl]-5-(2-oxoprop ylidene)-, (Z,E)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2(5H)-Furanone, 4-[2-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)ethenyl]-5-(2-oxoprop ylidene)-, (Z,E)-

There total 6 articles about 2(5H)-Furanone, 4-[2-(4-methoxy-2,6,6-trimethyl-1-cyclohexen-1-yl)ethenyl]-5-(2-oxoprop ylidene)-, (Z,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.3%

: 92510-21-9
9-carboxy-3-methoxy-β-ionylideneacetic acid anhydride

: 1439-36-7
1-triphenylphosphoranylidene-2-propanone

: 92510-15-1
4-[(E)-2-(4-Methoxy-2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-5-[2-oxo-prop-(Z)-ylidene]-5H-furan-2-one

: 92510-22-0
3-[(E)-2-(4-Methoxy-2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-5-[2-oxo-prop-(Z)-ylidene]-5H-furan-2-one

Guidance literature:: In benzene; for 2h; Heating;
DOI:10.1248/cpb.32.1709

Reference yield:

: 1209-67-2
3-methoxy-β-ionone

: 92510-15-1
4-[(E)-2-(4-Methoxy-2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-5-[2-oxo-prop-(Z)-ylidene]-5H-furan-2-one

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) ozone gas, 2.) zinc dust, 50 percent acetic acid / 1.) methanol, -20 degC, 3 h, 2.) methanol, room temperature, 1 h

2: 59 percent / piperidine / methanol / 27 h / Heating

3: 69 percent / 15 percent n-buthyl lithium / 1,2-dimethoxy-ethane; hexane / 3 h / Heating

4: 57 percent / 30 percent aq. H₂SO₄ / dioxane / 3.5 h / Heating

5: pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3.5 h / Heating

6: 11 percent / benzene / 2 h / Heating

With piperidine; n-butyllithium; sulfuric acid; ozone; acetic acid; pyridinium chlorochromate; zinc; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; hexane; dichloromethane; benzene;
DOI:10.1248/cpb.32.1709

Reference yield:

: 92510-11-7
3-methoxy-β-cyclocitral

: 92510-15-1
4-[(E)-2-(4-Methoxy-2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-5-[2-oxo-prop-(Z)-ylidene]-5H-furan-2-one

Guidance literature:: Multi-step reaction with 5 steps

1: 59 percent / piperidine / methanol / 27 h / Heating

2: 69 percent / 15 percent n-buthyl lithium / 1,2-dimethoxy-ethane; hexane / 3 h / Heating

3: 57 percent / 30 percent aq. H₂SO₄ / dioxane / 3.5 h / Heating

4: pyridinium chlorochromate (PCC) / CH₂Cl₂ / 3.5 h / Heating

5: 11 percent / benzene / 2 h / Heating

With piperidine; n-butyllithium; sulfuric acid; pyridinium chlorochromate; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; hexane; dichloromethane; benzene;
DOI:10.1248/cpb.32.1709