Benzenesulfonamide, N-[[(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[[[(4-methylphenyl)sulf onyl]oxy]methyl]-1,4-dioxan-2-yl]methyl]-4-methyl-

Base Information

Chemical Name:Benzenesulfonamide, N-[[(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[[[(4-methylphenyl)sulf onyl]oxy]methyl]-1,4-dioxan-2-yl]methyl]-4-methyl-
CAS No.:925425-51-0
Molecular Formula:C24H33NO9S2
Molecular Weight:543.659
Hs Code.:

Benzenesulfonamide,
N-[[(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[[[(4-methylphenyl)sulf
onyl]oxy]methyl]-1,4-dioxan-2-yl]methyl]-4-methyl-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzenesulfonamide, N-[[(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[[[(4-methylphenyl)sulf onyl]oxy]methyl]-1,4-dioxan-2-yl]methyl]-4-methyl-

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Technology Process of Benzenesulfonamide, N-[[(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[[[(4-methylphenyl)sulf onyl]oxy]methyl]-1,4-dioxan-2-yl]methyl]-4-methyl-

There total 4 articles about Benzenesulfonamide, N-[[(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[[[(4-methylphenyl)sulf onyl]oxy]methyl]-1,4-dioxan-2-yl]methyl]-4-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 925425-48-5
(2S,3R,5R,6R)-3-chloromethyl-5,6-dimethoxy-5,6-dimethyl[1,4]dioxane-2-methanol

: 925425-51-0
(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(p-toluenesulfonylamino)-methyl]-[1,4]-dioxan-2-ylmethyl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / dimethylformamide / 88 h / 80 °C

2: hydrogen / palladium on charcoal / methanol / 4 h / 20 °C / 258.57 Torr

3: 0.438 g / pyridine / CHCl₃ / 2.5 h / 0 °C

With pyridine; sodium azide; hydrogen; palladium on activated charcoal; In methanol; chloroform; N,N-dimethyl-formamide;

Reference yield:

: 173371-55-6
(2S,3S,5R,6R)-2,3-bis(hydroxymethyl)-5,6-dimethoxy-5,6-dimethyl<1,4>dioxane

: 925425-51-0
(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(p-toluenesulfonylamino)-methyl]-[1,4]-dioxan-2-ylmethyl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 4 steps

1: 47 percent / triphenylphosphine; pyridine; tetrachloromethane / CH₂Cl₂ / 23 h / 20 °C

2: sodium azide / dimethylformamide / 88 h / 80 °C

3: hydrogen / palladium on charcoal / methanol / 4 h / 20 °C / 258.57 Torr

4: 0.438 g / pyridine / CHCl₃ / 2.5 h / 0 °C

With pyridine; tetrachloromethane; sodium azide; hydrogen; triphenylphosphine; palladium on activated charcoal; In methanol; dichloromethane; chloroform; N,N-dimethyl-formamide; 1: Appel reaction;

Reference yield:

: 925425-49-6
(2S,3S,5R,6R)-3-azidomethyl-5,6-dimethoxy-5,6-dimethyl[1,4]dioxane-2-methanol

: 925425-51-0
(2S,3S,5R,6R)-5,6-dimethoxy-5,6-dimethyl-3-[(p-toluenesulfonylamino)-methyl]-[1,4]-dioxan-2-ylmethyl p-toluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on charcoal / methanol / 4 h / 20 °C / 258.57 Torr

2: 0.438 g / pyridine / CHCl₃ / 2.5 h / 0 °C

With pyridine; hydrogen; palladium on activated charcoal; In methanol; chloroform;