5,5-dimethyl-2-[(phenylamino)methylidene]cyclohexane-1,3-dione

Base Information

• Chemical Name: 5,5-dimethyl-2-[(phenylamino)methylidene]cyclohexane-1,3-dione
• CAS No.: 29974-49-0
• Molecular Formula: C15H17 N O2
• Molecular Weight: 243.305
• Hs Code.: 2922390090
• Mol file: 29974-49-0.mol

Synonyms:1,3-Cyclohexanedione,2-(anilinomethylene)-5,5-dimethyl- (7CI,8CI); 5,5-Dimethyl-2-(anilinomethylene)-1,3-cyclohexanedione

Chemical Property of 5,5-dimethyl-2-[(phenylamino)methylidene]cyclohexane-1,3-dione

Chemical Property:

• Vapor Pressure: 6.09E-06mmHg at 25°C
• Boiling Point: 378.9°Cat760mmHg
• Flash Point: 141.1°C
• PSA: 104.50000
• Density: 1.201g/cm³
• LogP: 5.01400

Purity/Quality:

99% ^*data from raw suppliers

2-(ANILINOMETHYLENE)-5,5-DIMETHYL-1,3-CYCLOHEXANEDIONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,5-dimethyl-2-[(phenylamino)methylidene]cyclohexane-1,3-dione

There total 9 articles about 5,5-dimethyl-2-[(phenylamino)methylidene]cyclohexane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

dimedone (126-81-8) + orthoformic acid triethyl ester (122-51-0) + aniline (62-53-3) → 2-(anilinomethylidene)-5,5-dimethylcyclohexane-1,3-dione (29974-49-0)

Guidance literature:

Reflux;

DOI:10.1016/j.poly.2019.114325

Reference yield: 80.0%

2-dimethylaminomethylene-5,5-dimethylcyclohexane-1,3-dione (75039-59-7) + aniline (62-53-3) → 2-(anilinomethylidene)-5,5-dimethylcyclohexane-1,3-dione (29974-49-0)

Guidance literature:

In ethanol;

DOI:10.1007/BF00479362

Reference yield: 78.0%

2-ethoxymethylidene-5,5-dimethylcyclohexane-1,3-dione + aniline (62-53-3) → 2-(anilinomethylidene)-5,5-dimethylcyclohexane-1,3-dione (29974-49-0)

Guidance literature:

In 1,4-dioxane; for 3h; Reflux;

DOI:10.1007/s00044-020-02579-4

upstream raw materials:

dimedone

N,N'-diphenylformamidine

orthoformic acid triethyl ester

aniline

Downstream raw materials:

2-formyl-5,5-dimethylcyclohexane-1,3-dione

N,N'-Bis-<(4,4-dimethyl-2,6-dioxocyclohexyliden)-methylen>-1,7-diamino-4-aza-heptan

2-deoxy-2-<(4,4-dimethyl-2,6-dioxocyclohexylidenemethyl)amino>-α,β-D-glucopyranose

N,N'-Bis-<(4,4-dimethyl-2,6-dioxocyclohexyliden)-methylen>-1,7-diamino-4-methyl-4-aza-heptan

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 29974-49-0 5,5-dimethyl-2-[(phenylamino)methylidene]cyclohexane-1,3-dione

Send

Send

Metric Ton KG G Pound L ML

Send

Send