Propanoic acid, 3-(tributylgermyl)-, cyclohexyl ester

Base Information

Chemical Name:Propanoic acid, 3-(tributylgermyl)-, cyclohexyl ester
CAS No.:925703-36-2
Molecular Formula:C21H42GeO2
Molecular Weight:399.153
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanoic acid, 3-(tributylgermyl)-, cyclohexyl ester

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Technology Process of Propanoic acid, 3-(tributylgermyl)-, cyclohexyl ester

There total 1 articles about Propanoic acid, 3-(tributylgermyl)-, cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 693-03-8
n-butyl magnesium bromide

: 14275-42-4
di-n-butylchlorogermane

: 3066-71-5,27458-65-7
cyclohexyl acrylate

: 925703-36-2
cyclohexyl 3-(tributylgermyl)propanoate

Guidance literature:: With triethyl borane; In tetrahydrofuran; diethyl ether; hexane; under N2 atm. Et3B in hexane and dry air were added to soln. Bu2GeClH and alkene in THF at 0°C, stirred for 10 min, warmed to room temp.,stirred for 10 h, BuMgBr in Et2O was added and stirred for 10 min; react. mixt. was poured into satd. aq. NH4Cl, extd. with t-BuOMe, dried over Na2SO4 and evapd., purification by chromy. on silica; elem. anal.;
DOI:10.1016/j.jorganchem.2006.04.043