Amylammoniumchlorid

Base Information

• Chemical Name: Amylammoniumchlorid
• CAS No.: 142-65-4
• Molecular Formula: C5H13 N . Cl H
• Molecular Weight: 123.626
• Hs Code.: 2921199090
• Mol file: 142-65-4.mol

Synonyms:Amylammoniumchlorid;SCHEMBL344840

Chemical Property of Amylammoniumchlorid

Chemical Property:

• Boiling Point: 105.5°Cat760mmHg
• Flash Point: 4.4°C
• PSA: 26.02000
• Density: 0.759g/cm³
• LogP: 2.68880
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 123.0814771
• Heavy Atom Count: 7
• Complexity: 19.9

Purity/Quality:

97% ^*data from raw suppliers

N-AMYLAMINEHYDROCHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCC[NH3+].[Cl-]

Technology Process of Amylammoniumchlorid

There total 9 articles about Amylammoniumchlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

pentanonitrile (110-59-8) → n-pentylamine hydrochloride (142-65-4)

Guidance literature:

With hydrogen; at 130 ℃; for 20h; under 750.075 Torr; chemoselective reaction;

DOI:10.1021/acscatal.0c04379

Reference yield: 92.0%

1-nitropentane (628-05-7) → n-pentylamine hydrochloride (142-65-4)

Guidance literature:

1-nitropentane; With C₃₆H₅₆Cl₃CrN₂O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 60 ℃; for 24h; Inert atmosphere; Schlenk technique;

With hydrogenchloride; In tetrahydrofuran; water; ethyl acetate; at 20 ℃;

DOI:10.1021/jacs.0c12318

Reference yield: 84.0%

Caproamide (628-02-4) → n-pentylamine hydrochloride (142-65-4)

Guidance literature:

Caproamide; With tetrafluoroboric acid; iodobenzene; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; at 25 ℃; for 48h; Inert atmosphere;

With hydrogenchloride; In dichloromethane; water; Inert atmosphere;

DOI:10.1039/c2cc16360h

upstream raw materials:

Caproamide

N-isopropylidene pentanamine

Tritylpentylamin

pentanonitrile

Downstream raw materials:

N-butylbenzamide