2,7-Dinitro-9-10-dihydrophenanthrene

Base Information

Chemical Name:2,7-Dinitro-9-10-dihydrophenanthrene
CAS No.:69533-68-2
Molecular Formula:C₁₄H₁₀N₂O₄
Molecular Weight:270.244
Hs Code.:
UNII:BBJ64LT564
DSSTox Substance ID:DTXSID60219792
Wikidata:Q27274581
Mol file:69533-68-2.mol

Synonyms:2,7-Dinitro-9-10-dihydrophenanthrene;Phenanthrene, 9,10-dihydro-2,7-dinitro-;2,7-Dinitro-9,10-dihydrophenanthrene;69533-68-2;BBJ64LT564;CCRIS 3376;9,10-Dihydro-2,7-dinitrophenanthrene;BRN 2151582;UNII-BBJ64LT564;DTXSID60219792;2,7-di-nitro-9,10-dihydrophenanthrene;Q27274581

Suppliers and Price of 2,7-Dinitro-9-10-dihydrophenanthrene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2,7-Dinitro-9-10-dihydrophenanthrene

Chemical Property:

Vapor Pressure:3.95E-08mmHg at 25°C
Boiling Point:457.8°C at 760 mmHg
Flash Point:228°C
PSA：91.64000
Density:1.424g/cm³
LogP:4.31500
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:270.06405680
Heavy Atom Count:20
Complexity:365

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2=C(C=CC(=C2)[N+](=O)[O-])C3=C1C=C(C=C3)[N+](=O)[O-]

Technology Process of 2,7-Dinitro-9-10-dihydrophenanthrene

There total 4 articles about 2,7-Dinitro-9-10-dihydrophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 776-35-2
9,10-dihydrophenanthrene

: 69533-68-2
2,7-dinitro-9,10-dihydrophenanthrene

Guidance literature:: With bismuth (III) nitrate pentahydrate; montmorillonite; In dichloromethane; for 0.0166667h; regioselective reaction; Microwave irradiation;

Reference yield: 71.0%

: 776-35-2
9,10-dihydrophenanthrene

: 69533-68-2
2,7-dinitro-9,10-dihydrophenanthrene

: 5329-87-3
2-nitro-9,10-dihydrophenanthrene

: 2,5-dinitro-9,10-dihydrophenanthrene

Guidance literature:: With nitric acid; acetic acid; at 0 - 5 ℃; for 6h;
DOI:10.1002/prac.19943360112

Reference yield:

: 776-35-2
9,10-dihydrophenanthrene

: 69533-68-2
2,7-dinitro-9,10-dihydrophenanthrene

: 5329-87-3
2-nitro-9,10-dihydrophenanthrene

: 17024-18-9
2-nitrophenanthrene

: rac-(4R^*,4aS^*,10aS^*)-4-nitro-1,2,3,4,4a,9,10,10a-octahydrophenanthren-4a-ol

: 2,5-dinitro-9,10-dihydrophenanthrene

Guidance literature:: With nitric acid; In acetic anhydride; at 5 ℃; for 24h; var. solvents, temp., reaction time, and HNO₃ concentration;
DOI:10.1007/BF01666094