2H-Tetrazole-2-acetic acid, 5-[[2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-[[(1,1-dimethylethyl)dimeth ylsilyl]oxy]-1-oxopropyl]amino]-, phenylmethyl ester, (S)-

Base Information

Chemical Name:2H-Tetrazole-2-acetic acid, 5-[[2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-[[(1,1-dimethylethyl)dimeth ylsilyl]oxy]-1-oxopropyl]amino]-, phenylmethyl ester, (S)-
CAS No.:92636-84-5
Molecular Formula:C24H38N6O6Si
Molecular Weight:534.688
Hs Code.:

2H-Tetrazole-2-acetic acid,
5-[[2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-[[(1,1-dimethylethyl)dimeth
ylsilyl]oxy]-1-oxopropyl]amino]-, phenylmethyl ester, (S)-

Synonyms:

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Chemical Property of 2H-Tetrazole-2-acetic acid, 5-[[2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-[[(1,1-dimethylethyl)dimeth ylsilyl]oxy]-1-oxopropyl]amino]-, phenylmethyl ester, (S)-

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Technology Process of 2H-Tetrazole-2-acetic acid, 5-[[2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-[[(1,1-dimethylethyl)dimeth ylsilyl]oxy]-1-oxopropyl]amino]-, phenylmethyl ester, (S)-

There total 3 articles about 2H-Tetrazole-2-acetic acid, 5-[[2-[[(1,1-dimethylethoxy)carbonyl]amino]-3-[[(1,1-dimethylethyl)dimeth ylsilyl]oxy]-1-oxopropyl]amino]-, phenylmethyl ester, (S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.0%

: 90181-27-4
[(S)-2-(tert-Butyl-dimethyl-silanyloxy)-1-(1H-tetrazol-5-ylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester

: 5437-45-6
Benzyl bromoacetate

: 92636-84-5
{5-[(S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionylamino]-tetrazol-2-yl}-acetic acid benzyl ester

: 92636-83-4
{5-[(S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionylamino]-tetrazol-1-yl}-acetic acid benzyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide;

Reference yield:

: 123254-10-4,90181-25-2
(2S)-2-tert-butoxycarbonylamino-3-(tert-butyldimethylsilanyloxy)propionic acid

: 92636-84-5
{5-[(S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionylamino]-tetrazol-2-yl}-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: N-methylmorpholine / tetrahydrofuran / 1 h / -15 °C

2: N-methylmorpholine

3: 59 percent / Et₃N / dimethylformamide

With 4-methyl-morpholine; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: C₁₉H₃₇NO₇Si

: 92636-84-5
{5-[(S)-2-tert-Butoxycarbonylamino-3-(tert-butyl-dimethyl-silanyloxy)-propionylamino]-tetrazol-2-yl}-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N-methylmorpholine

2: 59 percent / Et₃N / dimethylformamide

With 4-methyl-morpholine; triethylamine; In N,N-dimethyl-formamide;