5-Allyl-2,3-dimethoxy-N-(2-hydroxyethyl)benzamide

Base Information

Chemical Name:5-Allyl-2,3-dimethoxy-N-(2-hydroxyethyl)benzamide
CAS No.:26750-83-4
Molecular Formula:C₁₄H₁₉NO₄
Molecular Weight:265.309
Hs Code.:2924299090
Mol file:26750-83-4.mol

Synonyms:Benzamide,N-(2-hydroxyethyl)-2,3-dimethoxy-5-(2-propenyl)- (9CI); o-Veratramide,5-allyl-N-(2-hydroxyethyl)- (8CI); 2-Methoxy-3-methoxy-5-allyl-N-(b-hydroxyethyl)benzamide

Suppliers and Price of 5-Allyl-2,3-dimethoxy-N-(2-hydroxyethyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 5-Allyl-2,3-dimethoxy-N-(2-hydroxyethyl)benzamide

Chemical Property:

Vapor Pressure:1.08E-06mmHg at 25°C
Boiling Point:387.3°Cat760mmHg
Flash Point:188.1°C
PSA：71.28000
Density:1.123g/cm³
LogP:1.72920

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-Allyl-2,3-dimethoxy-N-(2-hydroxyethyl)benzamide

There total 5 articles about 5-Allyl-2,3-dimethoxy-N-(2-hydroxyethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 2-(5-allyl-2,3-dimethoxybenzylamino)ethanol

: 26750-83-4
5-allyl-N-(2-hydroxyethyl)-2,3-dimethoxybenzamide

Guidance literature:: With fluorenone imine; oxygen; In toluene; for 60h; Reflux;
DOI:10.1021/acs.joc.7b02630

Reference yield:

: 22934-51-6
5-allyl-2-hydroxy-3-methoxybenzaldehyde

: 26750-83-4
5-allyl-N-(2-hydroxyethyl)-2,3-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 12 h / Reflux

2: dichloromethane / 12 h / 20 °C / Molecular sieve

3: sodium cyanoborohydride / methanol / 4 h / 40 °C

4: fluorenone imine; oxygen / toluene / 60 h / Reflux

With fluorenone imine; oxygen; sodium cyanoborohydride; potassium carbonate; In methanol; dichloromethane; acetone; toluene;
DOI:10.1021/acs.joc.7b02630

Reference yield:

: 5-allyl-2,3-dimethoxybenzaldehyde

: 26750-83-4
5-allyl-N-(2-hydroxyethyl)-2,3-dimethoxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1: dichloromethane / 12 h / 20 °C / Molecular sieve

2: sodium cyanoborohydride / methanol / 4 h / 40 °C

3: fluorenone imine; oxygen / toluene / 60 h / Reflux

With fluorenone imine; oxygen; sodium cyanoborohydride; In methanol; dichloromethane; toluene;
DOI:10.1021/acs.joc.7b02630