4-amino-N,N-bis(2-chloroethyl)benzenesulfonamide hydrochloride (1:1)

Base Information

Chemical Name:4-amino-N,N-bis(2-chloroethyl)benzenesulfonamide hydrochloride (1:1)
CAS No.:25715-22-4
Molecular Formula:C10H14 Cl2 N2 O2 S . Cl H
Molecular Weight:333.6623
Hs Code.:

Synonyms:Benzenesulfonamide,4-amino-N,N-bis(2-chloroethyl)-, monohydrochloride (9CI); Sulfanilamide,N1,N1-bis(2-chloroethyl)-, monohydrochloride (8CI)

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-amino-N,N-bis(2-chloroethyl)benzenesulfonamide hydrochloride (1:1)

Chemical Property:

Vapor Pressure:1.46E-08mmHg at 25°C
Boiling Point:457.7°Cat760mmHg
Flash Point:230.6°C
Density:g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-amino-N,N-bis(2-chloroethyl)benzenesulfonamide hydrochloride (1:1)

There total 2 articles about 4-amino-N,N-bis(2-chloroethyl)benzenesulfonamide hydrochloride (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 17262-66-7
N,N-bis(2-chloroethyl)-4-(acetylamino)benzenesulfonamide

: 25715-22-4
sulfanilic acid-[bis-(2-chloro-ethyl)-amide]; hydrochloride

Guidance literature:: With hydrogenchloride; for 0.666667h; Heating;
DOI:10.1016/S0223-5234(01)01285-5

Reference yield:

: 121-60-8
p-acetylaminobenzenesulfonyl chloride

: 25715-22-4
sulfanilic acid-[bis-(2-chloro-ethyl)-amide]; hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / triethylamine / pyridine / 3 h / 38 - 42 °C

2: 92 percent / hydrochloric acid / 0.67 h / Heating

With hydrogenchloride; triethylamine; In pyridine;
DOI:10.1016/S0223-5234(01)01285-5