Cyclopropanecarboxamide, 1-(1,3-benzodioxol-5-yl)-N-[5-[(S)-(2-chlorophenyl)[[(R)-(1,1-dimethyleth yl)sulfinyl]amino]methyl]-2-thiazolyl]-

Base Information

• Chemical Name: Cyclopropanecarboxamide, 1-(1,3-benzodioxol-5-yl)-N-[5-[(S)-(2-chlorophenyl)[[(R)-(1,1-dimethyleth yl)sulfinyl]amino]methyl]-2-thiazolyl]-
• CAS No.: 926664-51-9
• Molecular Formula: C25H26ClN3O4S2
• Molecular Weight: 532.084

Synonyms:

Chemical Property of Cyclopropanecarboxamide, 1-(1,3-benzodioxol-5-yl)-N-[5-[(S)-(2-chlorophenyl)[[(R)-(1,1-dimethyleth yl)sulfinyl]amino]methyl]-2-thiazolyl]-

Chemical Property:

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Technology Process of Cyclopropanecarboxamide, 1-(1,3-benzodioxol-5-yl)-N-[5-[(S)-(2-chlorophenyl)[[(R)-(1,1-dimethyleth yl)sulfinyl]amino]methyl]-2-thiazolyl]-

There total 1 articles about Cyclopropanecarboxamide, 1-(1,3-benzodioxol-5-yl)-N-[5-[(S)-(2-chlorophenyl)[[(R)-(1,1-dimethyleth yl)sulfinyl]amino]methyl]-2-thiazolyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-benzo[1,3]dioxol-5-yl-cyclopropanecarbonyl chloride (945244-48-4) + (R)-N-(S)-1-(2-aminothiazol-5-yl)-1-(2-chlorophenyl)methyl-1,1-dimethylethylsulfmamide (926664-49-5) → (S)-N-(5-((R)-t-butylsulfinylamino-(2-chlorophenyl)methyl)thiazol-2-yl)-1-(benzo[d] [1,3]dioxol-5-yl)cyclopropanecarboxamide (926664-51-9)

Guidance literature:

With triethylamine; In dichloromethane; at 25 ℃; for 18h;

Reference yield: 72.0%

(S)-N-(5-((R)-t-butylsulfinylamino-(2-chlorophenyl)methyl)thiazol-2-yl)-1-(benzo[d] [1,3]dioxol-5-yl)cyclopropanecarboxamide (926664-51-9) → (S)-N-(5-(amino(2-chIorophenyl)methyl)thiazol-2-yl)-1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamide (926664-52-0)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol; at 25 ℃; for 1.5h;

upstream raw materials:

1-benzo[1,3]dioxol-5-yl-cyclopropanecarbonyl chloride

(R)-N-(S)-1-(2-aminothiazol-5-yl)-1-(2-chlorophenyl)methyl-1,1-dimethylethylsulfmamide

Downstream raw materials:

(S)-N-(5-(amino(2-chIorophenyl)methyl)thiazol-2-yl)-1-(benzo[d][1,3]dioxol-5-yl)cyclopropanecarboxamide

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