5-(1-Phenylpropyl)-1,2-dihydroacenaphthylene

Base Information

Chemical Name:5-(1-Phenylpropyl)-1,2-dihydroacenaphthylene
CAS No.:92669-84-6
Molecular Formula:C21H20
Molecular Weight:272.39
Hs Code.:
DSSTox Substance ID:DTXSID90537870

Synonyms:92669-84-6;5-(1-PHENYLPROPYL)-1,2-DIHYDROACENAPHTHYLENE;DTXSID90537870

Suppliers and Price of 5-(1-Phenylpropyl)-1,2-dihydroacenaphthylene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(1-Phenylpropyl)-1,2-dihydroacenaphthylene

Chemical Property:

XLogP3:6.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:272.156500638
Heavy Atom Count:21
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC(C1=CC=CC=C1)C2=CC=C3CCC4=C3C2=CC=C4

Technology Process of 5-(1-Phenylpropyl)-1,2-dihydroacenaphthylene

There total 5 articles about 5-(1-Phenylpropyl)-1,2-dihydroacenaphthylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 92669-70-0,92669-71-1
5-(1-phenyl-1-propenyl)-acenaphthene

: 92669-84-6
5-(1-phenyl-1-propyl)acenaphthene

Guidance literature:: With hydrogen; palladium on activated charcoal; In benzene; for 48h; under 1810.02 Torr;
DOI:10.1021/jo00198a011

Reference yield:

: 51754-77-9
1-acenaphthenyl(diisobutyl)aluminum

: 92669-84-6
5-(1-phenyl-1-propyl)acenaphthene

Guidance literature:: Multi-step reaction with 4 steps

1: 10 percent Spectr_. / heptane; diethyl ether / 22 h / 70 °C

2: 72 percent / AlCl₃ / CS₂ / 5 h / 25 °C

3: 2) p-toluenesulfonic acid / 1) ether 2) benzene, reflux

4: H₂ / Pd/C / benzene / 48 h / 1810.02 Torr

With aluminium trichloride; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In carbon disulfide; diethyl ether; n-heptane; benzene;
DOI:10.1021/jo00198a011

Reference yield:

: 55720-25-7
5-propionylacenaphthene

: 92669-84-6
5-(1-phenyl-1-propyl)acenaphthene

Guidance literature:: Multi-step reaction with 2 steps

1: 2) p-toluenesulfonic acid / 1) ether 2) benzene, reflux

2: H₂ / Pd/C / benzene / 48 h / 1810.02 Torr

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In benzene;
DOI:10.1021/jo00198a011