(8S)-8α,13β-Dihydroxyserratinane-5-one

Base Information

• Chemical Name: (8S)-8α,13β-Dihydroxyserratinane-5-one
• CAS No.: 5545-99-3
• Molecular Formula: C₁₆H₂₅NO₃
• Molecular Weight: 279.379
• Mol file: 5545-99-3.mol

Synonyms:Decahydro-1,4-dihydroxy-2-methyl-5H,9H,12H-indeno(7a,1-h)indolizin-12-one;(8alpha,13S)-8,13-Dihydroxyserratinan-5-one;

Chemical Property of (8S)-8α,13β-Dihydroxyserratinane-5-one

Chemical Property:

• Melting Point: 244-5°C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 66.73000
• Density: g/cm³
• LogP: 1.95240

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Description: A further alkaloid present in Lycopodium serratum Thunb. vaT. thunbergii Mak. The base crystallizes from Me2CO in colourless prisms and has [α]8D - 27.8° (c 1.44, EtOH). Two non-phenolic hydroxyl groups are present and the alkaloid forms the 8-0-acetate, m.p. 244-5°C; the l3-0-acetate, m.p. 240-2°C and the di-O-acetate, m.p. 1 57-8°C. The tetracyc1ic structure has been proposed on the basis of the mass spectra of the alkaloid and a tentative biogenesis from lycodoline-type alkaloids also proposed.

Technology Process of (8S)-8α,13β-Dihydroxyserratinane-5-one

There total 5 articles about (8S)-8α,13β-Dihydroxyserratinane-5-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (+/-)-Serratinin (5545-99-3,25441-11-6,55856-79-6,55885-96-6)

Guidance literature:

entspr. Triketon (10), NaBH4;

DOI:10.1039/C39740000827

Reference yield:

→ dl-8-Episerratinin (5545-99-3,25441-11-6,55856-79-6,55885-96-6)

Guidance literature:

'Triketon' 18, NaBH4 (Red.);

Reference yield:

→ Serratinin (5545-99-3,25441-11-6,55856-79-6,55885-96-6)

Guidance literature:

Monoacetylserratinin;

DOI:10.1016/S0040-4039(00)75731-5

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